Metrohm 830 Instructions For Use Manual
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Metrohm 830 Instructions For Use Manual

Metrohm 830 Instructions For Use Manual

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830 IC Interface
Instuctions for Use
CH-9101 Herisau/Switzerland
E-Mail
info@metrohm.com
8.830.1003
Internet
www.metrohm.com

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  • Page 1 830 IC Interface Instuctions for Use CH-9101 Herisau/Switzerland E-Mail info@metrohm.com 8.830.1003 Internet www.metrohm.com...
  • Page 3 CH-9101 Herisau/Switzerland E-Mail info@metrohm.com Internet www.metrohm.com 830 IC Interface 5.830.0020 Program Instructions for Use 8.830.1003 07.2003 / pkl...
  • Page 4 Teachware Metrohm AG Oberdorfstrasse 68 CH-9101 Herisau teachware@metrohm.com Edition 2003 These instructions are protected by copyright. All rights reserved. Although all the information given in these instructions has been checked with great care, errors cannot be entirely excluded. Should you notice any mistakes please inform the author at the...

  • Page 5: Table Of Contents

    828 IC Dual Suppressor ..............24 2.4.15 837 IC Combi Degasser..............25 3 Operation ............26 Switch instrument on/off ............26 Settings in the "830 IC Interface" window......27 3.2.1 Event output lines ................30 4 Appendix ............34 Technical data................. 34 Scope of delivery ..............38 Optional accessories ..............
  • Page 6 4.5.3 Quality Management Principles ..........43 Index ..................44 List of illustrations Fig. 1: Connection possibilities at 830 IC Interface ..........1 Fig. 2: Front of 830 IC Interface ................2 Fig. 3: Rear of 830 IC Interface................3 Fig. 4: Connection of 830 IC Interface to PC............

  • Page 7: Introduction

    IC or HPLC peripheral instruments. Up to 16 instruments includ- ing 4 detectors can be connected to the 830 IC Interface and controlled by means of the «IC Net» PC software. The 830 IC Interface can also record and convert the analog signals from a maximum of 4 channels (two at once) which are processed at very high resolution.

  • Page 8: Parts And Controls

    Parts and controls In this section you will find the numbers and designations of the parts and controls of the 830 IC Interface. The numbering applies through- out the instructions for use, i.e. bold numbers in the text (e.g. ) refer to the parts and controls illustrated here.

  • Page 9: Fig. 3: Rear Of 830 Ic Interface

    12 Remote input/output lines connec- tion (RUN) 6 PC connection RS232 interface 13 Remote input/output lines connec- tion (COM) System 1 14 RS232 interfaces 7 Analog signal connection 8 Remote input/output lines connec- tion (RUN) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 10: Information On The Instructions For Use

    Information on the Instructions for Use Please read through these Instructions for Use carefully before you put the 830 IC Interface into operation. The Instructions for Use contain information and warnings to which the user must pay attention in order to assure safe operation of the instrument.

  • Page 11: Notation And Pictograms

    Attention This symbol indicates important information that you should read before continuing. Information This symbol indicates additional information and tips which may be of particular use to you. 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 12: Safety Notes

    1 Introduction Safety notes While electrical safety in the handling of the 830 IC Interface is assured in the context of the specifications IEC 1010-1 (protection class 1, de- gree of protection IP40), the following points should be noted: • Mains connection The mains connection must be effected in accordance with the instructions in section 2.2.

  • Page 13: Installation

    Arrangement of the instruments The modular IC instruments can be piled up in any order. The best place for the 830 IC Interface is on top of a modular IC system. The 830 IC Interface should always be placed above components carrying liquids so that any leaks which may occur in the tubing or connections cannot cause damage by leakage of liquids (e.g.

  • Page 14: Mains Connection

    2 (protection class 1). Any break in the earthing inside or outside the instrument can make it a hazard! Plug the mains cable into mains connection plug 5 at the 830 IC Inter- face (see Fig. 3). 2.2.3...

  • Page 15: Connection To The Pc

    Always switch off 830 IC Interface and PC before you connect the two instruments with the 6.2134.100 Cable Connect the PC connection 6 at the 830 IC Interface to one of the serial COM ports at the PC using the 6.2134.100 Cable (9 pin/9 pin). If only a 25-pin COM interface is available on the PC then the 6.2125.110...

  • Page 16: Connection Of External Instruments

    Before an external instrument is connected to the 830 IC Interface, the 830 IC Interface must always be switched off using mains switch Each system of the two versions of the 830 IC Interface has four RS232 interfaces 10 or 14 for connection of a maximum of 8 external instru-...
  • Page 17 • 761 Compact IC: This instrument is already pre-configured, no additional set- tings must be made. • 750 IC Autosampler: Always switch on the 830 IC Interface first and then the 750 Autosampler. • 766 IC Sample Processor: >RS232 settings...

  • Page 18: 819 Ic Detector, 820 Ic Separation Center, 818 Ic Pump

    • 2.820.0210 820 IC Separation Center with 1 injector and column heater • 2.818.0110 818 IC Pump 6.2134.130 6.2125.090 6.2115.070 6.2134.100 6.2134.040 6.2134.090 Interconncection Fig. 5: Connection of 819, 820 and 818 (MIC 1) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 19: 833 Ic Liquid Handling Pump Unit

    • 2.818.0110 818 IC Pump • 2.833.0010 833 IC Liquid Handling Pump Unit 6.2134.130 6.2125.090 6.2115.070 6.2134.100 6.2134.040 6.2134.090 6.2128.180 Interconnection Fig. 6: Connection of 820, 819, 818 and 833(Pump Unit) (MIC 2) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 20: 833 Ic Liquid Handling Suppressor-Unit

    819-1 6.2134.130 6.2125.090 6.2115.070 6.2115.070 819-2 6.2125.090 818-2 6.2134.100 818-1 6.2134.040 6.2143.200 6.2134.090 6.2134.090 6.2128.180 × × Fig. 7: Connection of 2 819, 820, 2 818 and 833 (Suppressor Unit) (MIC 3) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 21: 833 Ic Liquid Handling Sample Prep Unit

    6.2134.040 833 Sample Prep B (LOOP) A (PCC) 6.2128.180 6.2128.180 833 Suppressor 6.2115.070 6.2134.100 833 Pump 6.2128.180 6.2134.090 6.2134.090 Fig. 8: Connection of 833 (Sample Prep Unit) to MIC 6 for Neutralization 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 22: 833 Ic Liquid Handling Dialysis Unit

    • 2.833.0040 833 IC Liquid Handling Dialysis Unit Interconnection 6.2134.130 6.2143.220 6.2125.090 6.2115.070 833 Dialysis 6.2134.100 833 Suppressor 6.2134.040 6.2134.090 Fig. 9: Connection of 819, 820, 818, 833 (Suppressor Unit) and 833 (Dialysis Unit) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 23: 833 Ic Liquid Handling Ultra Filtration Unit

    • 2.833.0050 833 IC Liquid Handling Ultra Filtration Unit Interconnection 6.2134.130 6.2143.220 6.2125.090 6.2115.070 833 Ultra Filtration 6.2134.100 833 Suppressor 6.2134.040 6.2134.090 Fig. 10: Connection of 819, 820, 818, 833 (Suppressor Unit) and 833 (Ultra Filtration Unit) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 24: Triathlon Autosampler

    • 2.820.0210 820 IC Separation Center 820 with 1 injector and column heater • 2.818.0110 818 IC Pump • 2.135.0100 Triathlon Autosampler Interconnection 6.2134.130 6.2125.090 6.2115.070 Triathlon 6.2134.100 6.2134.040 6.2134.090 6.2134.000 Fig. 11: Connection of 819, 820, 818 and Triathlon 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 25: 766 Ic Sample Processor

    • 2.820.0210 820 IC Separation Center 820 with 1 injector and column heater • 2.818.0110 818 IC Pump • 2.766.0010 766 IC Sample Processor Interconnection 6.2134.130 6.2125.090 6.2115.070 6.2134.100 6.2134.040 6.2134.090 6.2134.080 6.2141.110 Fig. 12: Connection of 819, 820, 818 and 766 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 26: 791 Ic Va Detector

    • 2.820.0210 820 IC Separation Center with 1 injector and column heater • 2.818.0110 818 IC Pump • 2.791.0020 791 IC VA Detector Interconnection 6.2134.130 6.2125.090 6.2115.070 6.2134.100 6.2134.040 6.2134.090 6.2128.130 Fig. 13: Connection of 819, 820, 818 and 791 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 27: 761 Compact Ic

    2.4 Connection of external instruments 2.4.11 761 Compact IC Example Connection of a modular system and a 761 Compact IC to a 830 IC In- terface (if not enough COM ports are available at the PC). Instruments • 2.830.0020 830 IC Interface •...

  • Page 28: 812 Ic Valve Unit And 817 Bioscan

    Modular system for sugar analysis. Instruments The setup of the instruments corresponds to the Modular IC System 8 (MIC 8 Advanced) enhanced by the 830 IC Interface. • 2.830.0020 830 IC Interface • 2.817.0010 817 Bioscan • 2.812.0010 812 IC Valve Unit 812 with 1 valve •...

  • Page 29: 816 Ic Eluent Selector

    • 2.818.0110 818 IC Pump • 2.816.0010 816 IC Eluent Selector Interconnection 6.2134.130 6.2125.090 6.2115.070 6.2134.100 6.2134.040 6.2134.090 6.2134.080 Fig. 16: Connection to 819, 820, 818 and 816 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 30: 828 Ic Dual Suppressor

    • 2.818.0110 818 IC Pump, 2 devices • 2.828.0010 828 IC Dual Suppressor 6.2134.100 6.2134.130 6.2125.090 6.2134.040 6.2115.070 6.2128.180 6.2134.090 6.2134.080 Interconnection Fig. 17: Connection to 819, 820, 2x818 and 828 (MIC 10) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 31: 837 Ic Combi Degasser

    • 2.818.0010 818 IC Pump • 2.837.0030 837 IC Combi Degasser Interconnection 6.2134.130 6.2125.090 6.2115.070 6.2134.100 6.2134.040 6.2134.090 6.2128.180 Fig. 18: Connection to 819, 820, 818 and 837 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 32: Operation

    «IC Net» Instructions for Use and to the on-line help in the PC pro- gram. Switch instrument on/off The 830 IC Interface is switched on and off using mains switch 3 on the rear of the instrument (see Fig. 3). After the instrument has been switched on a self-test is running. The...

  • Page 33: Settings In The "830 Ic Interface" Window

    3.2 Settings in the "830 IC Interface" window Settings in the "830 IC Interface" window By clicking the 830 icon in the toolbar with the left mouse button or by clicking this icon with the right mouse button and selecting the...
  • Page 34 Display of the software handshake mode. Handshake Display of the intermediate memory in byte. FIFO size The values are displayed correctly only if the 830 IC Interface is con- nected and switched on. 830 IC Interface / 8.830.1003 Instructions for Use...
  • Page 35 3.2 Settings in the "830 IC Interface" window Links tab of the is used for RS232 interface (COM Links 830 IC Interface port) selection and settings. Name of the instrument. Alias If this entry is clicked with the right mouse but-...

  • Page 36: Event Output Lines

    Program 830 System [#] program for the event output lines of the 830 IC Interface can be en- tered. This program is started automatically as defined in the Start mode window either at the moment the determination is started (...
  • Page 37 3.2 Settings in the "830 IC Interface" window Program On the subpage, program steps including time, program in- Program struction and parameter can be entered. Time at which program instruction is applied. Erste Spalte Entry range: 0.0 ... 999.9 min...
  • Page 38 Add new remote command. <Add> Delete selected remote command. <Delete> Activate the defined remote commands for in- <Activate> sertion into the time program. 830 IC Interface / 8.830.1003 Instructions for Use...
  • Page 39 830 System [#] values for the seven event output lines of system 1 or system 2 of the 830 IC Interface. These startup values are sent each time the system is connected or a determination is started. Each event output line can be set to the following values:...

  • Page 40: Appendix

    4 Appendix 4 Appendix Technical data Provided that nothing to the contrary is mentioned, the published data are typical values for the 830 IC Interface at an ambient temperature of 25°C. Mains connection Voltage 100...240 V Frequency 50...60 Hz Power consumption 2 ×...
  • Page 41 30 V / 1 A DC Input lines 1 digital input per system for external method start. 470k Ext. Start Maximum load for external contact: approx. 0.1 mA at max. cut-off voltage of approx. 830 IC Interface / 8.830.1003 Instructions for Use...
  • Page 42 Immunity to interference Standards met: - EN/IEC 61326 - EN/IEC 61000-4-2 - EN/IEC 61000-4-3 - EN/IEC 61000-4-4 - EN/IEC 61000-4-5 - EN/IEC 61000-4-6 - EN/IEC 61000-4-8 - EN/IEC 61000-4-11 - EN/IEC 61000-4-14 - NAMUR 830 IC Interface / 8.830.1003 Instructions for Use...
  • Page 43 Polyurethane rigid foam (PUR) with fire protection for fire class UL94VO, CFC-free Material of base Steel, enameled Dimensions Width 260 mm Height 130 mm Depth 340 mm Weight (with accessories) 4.8 kg 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 44: Scope Of Delivery

    4 Appendix Scope of delivery Subject to changes ! The 830 IC Interface 2.830.0020 for 2 IC systems includes the following parts: Quant. Order-No. Description 6.2115.070 Remote Connection cable Connection cable 830 IC Interface – 820 IC Separation Center 6.2134.130 Connection cable Connection cable 830 IC Interface –...

  • Page 45: Optional Accessories

    Connection cable 830 IC Interface – 1 external device (818, 819, 766, etc.) 6.2141.110 Connection cable Connection cable 830 IC Interface – 819 IC Detector– 766/788 IC Sample Processor (accessory part of 766/788) 830 IC Interface / 8.830.1003 Instructions for Use...

  • Page 46: Validation / Glp

    Procedures (SOP)». This SOP can be adapted for your ion chromatography system and used for its validation. The 830 IC Interface must be included as a part of the whole ion chro- matography system, whose most important components include the pumps, separation columns, detector and evaluation system, in the all- embracing validation of the whole system.

  • Page 47: Warranty And Conformity

    Metrohm from any liability to pay compensation. If any instruments and parts have to be returned, the original packaging should be used if at all possible.

  • Page 48: Declaration Of Conformity

    EN 61010-1 Safety requirements for electrical equipment for measurement, control and laboratory Metrohm Ltd. is holder of the SQS-certificate of the quality system ISO 9001 for quality assurance in design/development, production, installation and servicing. The system software, stored in Read Only Memories (ROMs) has been validated in connection with standard operating procedures in respect to functionality and performance.

  • Page 49: Quality Management Principles

    Metrohm Ltd. holds the ISO 9001 Certificate, registration number 10872-02, issued by SQS (Swiss Association for Quality and Management Systems). Internal and external au- dits are carried out periodically to assure that the standards defined by Metrohm’s QM Manual are maintained.

  • Page 50: Index

    Installation........7 .........29 Change 817 Bioscan Instructions for Use Connection to 830 ....22 Check ..........7 830 IC Interface 8.830.1003 .4, 38 Settings ........10 ..........29 COM # Autodatabase 8.110.8213..39 818 IC Pump Compliance White Paper IC Cap 1.0 8.110.8303 .....38 Connection to 830 ....
  • Page 51 Warning .......... 5 Technical Data......35 Technical Data......34 Warranty ........41 RS232 interface 14 Pictograms ........5 Figure......... 3 Power consumption .....34 Technical Data......35 ........30, 31 Program RS232 parameters....... 28 Program instruction ......31 830 IC Interface / 8.830.1003 Instructions for Use...

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