Katanax FLUXPENSER XFP-01 Manual

Automatic flux dispenser

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XFP-01
FLUXPENSER
®
Automatic flux dispenser

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Summary of Contents for Katanax FLUXPENSER XFP-01

  • Page 1 XFP-01 FLUXPENSER ® Automatic flux dispenser...
  • Page 3 Thank you for having chosen the XFP-01 flux dispenser from Katanax. To enjoy years of reliable, efficient and safe use of this time-saving instrument, please read this manual thoroughly and keep it in a safe and handy place for future reference.
  • Page 4: Table Of Contents

    Introduction .................. 13 Flux weighing basics ................13 Automatic dispensers ................13 The XFP-01 .................... 14 Main features of the Katanax XFP-01 ............15 How the unit works ..............16 Dispensing modes .................. 16 Using the XFP-01 (basic) ............. 17 The main running screen ................
  • Page 5 Warranty ..................27 Contacting Katanax ..............28...
  • Page 6: Installation

    Congratulations on your acquisition of the XFP-01 flux dispenser, from Katanax. Please read the following section for proper commissioning of your instrument. Do not hesitate to contact Katanax with any question you might have with this crucial step. Box contents The instrument comes with its essential accessories.
  • Page 7: Parts Nomenclature

    Parts nomenclature Base: Head compartment: Head compartment post:...
  • Page 8 Base post: Weighing post: Spill plate:...
  • Page 9: Assembly Instructions

    Crucible holder: Assembly instructions To assemble the XFP-01, follow these steps: Screw the Base post into the Base.
  • Page 10 Screw the Head compartment post in the Head compartment. Thread the Head compartment cable into the Base post and Base. Adjust the height Install this assembly on the provided rubber mat, on a stable, vibration- free table.
  • Page 11 Locate and identify the connectors at the back of the control unit: Connect the mechanical head compartment cable (5-conductor) into connector A. Connect the balance connection cable (6-conductor) into connector B. Connect the power supply into connector D. 10. Follow the scale manufacturer’s instructions to assemble the analytical balance.
  • Page 12 11. On the scale weighing sensor, carefully lay the weighing post: 12. Then place the spill plate: 13. And finally the crucible holder :...
  • Page 13: Questions

    14. Your setup should now look like this: 15. Flip the switch C to turn the unit on. Questions ? Should you have any question regarding the proper installation and start-up of your instrument, please contact Katanax directly (see information on page 28) for assistance.
  • Page 14: Precautions

    Some flux types are made up of spherical micro-beads, which are very slippery when spilled on a floor. Promptly clean up any flux spill to prevent hazardous situations. Original accessories For your safety, use only the original power supply and Katanax-approved peripherals to this equipment.
  • Page 15: Introduction

    Introduction This section intends to introduce the reader to basic dispensing techniques and to familiarize him or her to the XFP-01. Flux weighing basics When preparing samples for XRF by fusion, the spectrometer will measure the concentration of the sample atomic components in the flux matrix. This means that the matrix itself must be accurately known and prepared.
  • Page 16: The Xfp-01

    The XFP-01 General view Enter the XFP-01, the flux weighing machine that combines the accuracy of an analytical balance with the convenience of an automatic dispensing system. LCD screen Keypad The LCD screen and keypad Upon turning the instrument on, the system will boot up and be ready to accept commands from the user.
  • Page 17: Main Features Of The Katanax Xfp-01

    Handshake: No Handshake If the scale was provided with the flux dispenser, these parameters have been adjusted in factory. Otherwise, your balance must be pre-registered in the Balance Menu. Main features of the Katanax XFP-01 Accuracy  Real-time weight display Safety ...
  • Page 18: How The Unit Works

    How the unit works Dispensing modes This instrument offers two (2) very different operation modes. The choice of the mode will depend on internal laboratory procedures, as well as on the type of intended analysis. Fixed-weight mode When preparing a sample for fusion, the laboratory protocols often call for a fixed amount of sample, to be mixed with a fixed amount of flux.
  • Page 19: Using The Xfp-01 (Basic)

    Using the XFP-01 (basic) The main running screen After turning the unit on, the following display will appear, allowing the user to change parameters or start a dispensing. Amount of flux and sample to Today’s market has seen a proliferation of various mold diameters. Consequently, one must adapt the amount of flux and sample to obtain a full disk that will not overflow out of the mold.
  • Page 20: Installing The Crucible

    Our recommendation is to measure the actual inner diameter on the bottom of the mold and apply the following formula, to obtain the total mass of sample and flux: (Mold diameter [mm])² Total mass [g] = Thus, for a 32-mm inner diameter mold (recommended diameter), we obtain 32²...
  • Page 21 In the end, the screen shows the message: “Done !” Done ! ~ 008.0000 g Remove the dosed crucible. Wait for the message saying to Add the container before installing the next one. If the same weight is used for the next dispensing, no further action will be required than installing the crucible or the container.
  • Page 22: Manual Mixing

    Manually add the sample into the crucible. (Leave the crucible on the balance.) Confirm the sample mass with the “Enter/Right arrow” button; Again, the instrument will record the mass of sample. It will then multiply this amount with the requested ratio to obtain the total mass of flux needed. However, since a pre-weighing has been done, that mass will be subtracted to obtain the final amount to be added.
  • Page 23: A Complete Dispensing Procedure

    A complete dispensing procedure Turn the units on (scale and dispenser) Make sure the balance is in standard weighing mode. (On a Vibra scale, use the Function button to toggle modes.) Select the appropriate dispensing mode (fixed-weight or ratio) Set the current weight (or ratio) and press Enter Follow instructions on display and wait for the process to be completed Manually mix the flux with the sample, as needed Add other reagents, as needed...
  • Page 24: Advanced Parameters

    Advanced parameters When a specific flux type does not seem to be easily dispensed by the unit with the preset parameters, it is necessary to manually edit those, to optimize accuracy and dispensing times. Accessing the “hidden” advanced parameters Once dispensing parameters are optimized for a given flux type, they should normally not be tampered with.
  • Page 25 The respective basic parameters for those two main flux types for your specific unit (s/n #_________________) are as follows: Micro-bead Granular Flux type: (spherical) (crystalline) 1 Base Duty 2 Fine Thold. 3 Vib. Thold. 4 Vib. Tries 5 Step.size 6 Serial Out LIMS 7 Prep.revs If you find that the basic parameters could use some further optimization, here is...
  • Page 26: Buzzer

    Serial Out This parameter allows selecting the output mode of the XFP-01. The default mode is LIMS. The other modes are reserved for manufacture use. Prep. revs This represents the number of spring auger rotations before the user is prompted to add the sample, in ratio mode.
  • Page 27: Service Operations

    Service operations This section describes tasks that are performed on a regular basis, and are performed to adjust or repair a malfunctioning system of the instrument. Balance communication test To verify if the dispensing unit is communicating properly with the balance, press the PRINT button on the balance;...
  • Page 28: Technical Specifications

    Technical specifications Electrical Power supply input ........100-240VAC, 50-60 Hz Power supply output ......... 12 VDC, 2.5A Physical Total weight....6 kg (13 lbs) Weighing unit: Width ......20 cm (8 in) Depth ......45 cm (18 in) Controller: Width ......20 cm (8 in) Depth ......
  • Page 29 Katanax reserves the right to make changes in the design or to make additions or improvements with respect to its product without incurring any obligation to...
  • Page 30 Contacting Katanax Katanax sales and technical staff can be reached at the following address: Katanax inc. 2500, Jean-Perrin, suite 100 Quebec, QC Canada G2C 1X1 Tel.: (+1) 418-915-4848 E-mail: info@katanax.com Web: www.katanax.com When contacting us, kindly have the serial number of the instrument at hand.

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