Biotage TurboVap 96 User Manual

Biotage TurboVap 96 User Manual

Concentration workstation

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TurboVap 96
Concentration Workstation
User's Manual

Copyright 2010, Biotage AB. All rights reserved.
P/N 128097 Rev. 00

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Summary of Contents for Biotage TurboVap 96

  • Page 1 TurboVap 96  Concentration Workstation User’s Manual  Copyright 2010, Biotage AB. All rights reserved. P/N 128097 Rev. 00...
  • Page 2: Preface

    WARNINGS • The TurboVap 96 is NOT designed for in vitro testing or for use with highly corrosive acids. • To reduce the risk of electric shock, do not remove the cover. No user serviceable parts are inside.
  • Page 3 Preface Product Safety Warning The TurboVap 96 power switch is the same type of power switch used on most laboratory equipment such as gas chromatographs, spectrophotometers, liquid chromatographs, and computers. The TurboVap products are safely used in the laboratory when “Good Laboratory Practices” are followed as with any other lab equipment.
  • Page 4 Service and Customer Support Plans Biotage offers a full range of services to ensure your success. From our original factory warranty through a comprehensive line of customer support plans, Biotage AB offers you Field Service Engineers and In-house Specialists who are dedicated to supporting your hardware, software and application development needs.
  • Page 5 Crush hazard. Risk of body parts, hair, jewelry, or clothing getting caught in a moving part. Danger d’écrasement. Faire attention que les parties corporelles, les cheveux, les bijoux ou les vêtements ne soient pas pris dans une pièce mobile. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 6 Signifie que l’appareil a réussi les tests de sécurité pour la mise à la terre, le courant transitoire de ligne d’alimentation et la perte de courant. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 7 Mandatory action Green Safe condition or information Les étiquettes de l’appareil Jaune Attention, danger potentiel sont codées Rouge Arrêter couleur: Bleu Intervention obligatoire Vert Condition sûre ou informations de sécurité P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 8: Table Of Contents

    Multiple Sample Processing ................12 Microplates and Deepwell Plates ............... 12 Hardware ....................... 13 TurboVap 96 - Front ..................13 TurboVap 96 - Cover Open ................14 TurboVap 96 - Rear................... 15 TurboVap 96 - Left Side ..................16 Microplate Adapter .................... 16 Front Panel .......................
  • Page 9 Long Term Storage ................... 36 Troubleshooting ....................37 Troubleshooting the Concentration ..............37 Troubleshooting the Front Panel Display ............38 Workstation Not Operational ................39 Specifications ....................... 40 Index ........................43 P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 10: Introduction

    Figure 1. TurboVap 96 Gas Vortex Shearing Action The TurboVap 96 uses a patented “gas vortex shearing action” to maintain high evaporation rates under mild thermal conditions. When you close the cover, 96 gas nozzles in the manifold align with each well of the microplate or deepwell plate.
  • Page 11: Microplate Heating

    Vapor Removal The solvent vapors are removed by a blower at the front of the TurboVap 96 that blows air across the top of the microplates and through the exhaust port at the back of the workstation. From the exhaust port, the venting hose must be routed to a suitable outside ventilation system.
  • Page 12: Requires No Exhaust Hood

    Deepwell plates are placed directly on the surface of the locator plate. Microplates use the supplied adapter to position the top of the microplate at the same level as the top of a deepwell plate. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 13: Hardware

    Front Panel Position 2 Position 1 Regulator Regulator Figure 3. TurboVap 96 Hardware, Front View Front Panel Controls the setup and operation of the Concentration Workstation. “Front Panel” on page 17 for details. Cover Holds the gas manifold that directs the gas into the wells of each plate to create the gas vortex shearing action.
  • Page 14: Turbovap 96 - Cover Open

    Microplate Adapter Plate Locations Heater Figure 4. TurboVap 96 with Cover Open Gas Manifolds Each manifold consists of 96 individual gas nozzles, which fit inside each microplate well. Each nozzle supplies gas to concentrate the sample in one microplate well.
  • Page 15: Turbovap 96 - Rear

    Gas Inlet Exhaust Power Port Entry Port Figure 5. TurboVap 96 Hardware, Rear View Alarm Volume Control Adjusts the loudness of the beeper. Service Panel Used by service personnel to access the exhaust blower and the sensor/interconnect module. Quick-disconnect Gas Inlet Connects the gas supply to the workstation.
  • Page 16: Turbovap 96 - Left Side

    Hardware TurboVap 96 - Left Side Position 1 Power Switch Regulator Figure 6. TurboVap 96 Hardware, Left Side View Power Switch Turns the power on and off. Microplate Adapter Figure 7. Microplate Adapter Microplate Adapter Used to raise microplates up to the proper height. Not used with deepwell plates.
  • Page 17: Front Panel

    Hardware Front Panel Figure 8. TurboVap 96 Front Panel Display Indicator Lights Indicate which setting is displayed in the Value and Units displays. Gas Time - displays the length of time to evaporate, from 1 to 99 minutes. 00 evaporates until manually stopped.
  • Page 18 If the flow rate drops below 5 SCFH when the evaporation is in process, the Low Flow LED lights and the alarm beeps continuously. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 19: Installation

    Installation Installation This section describes how to unpack the TurboVap 96, how to prepare the site, and how to install the TurboVap 96. Unpacking the TurboVap 96 Unpack the shipping container and verify that all parts listed below are included. If any part is damaged or missing, contact Biotage (see “Contact Biotage 1-Point Support”...
  • Page 20: Site Preparation

    Installation Site Preparation Before installing the TurboVap 96 Concentration Workstation, you must have an appropriate location with available gas and electrical sources and adequate ventilation as specified by these site preparation requirements. Space Minimum bench space needed for the Concentration workstation and any accessories: •...
  • Page 21 Line 50 - 60 Hz 50 - 60 Hz Frequency Fuse (1) 6A, F250V (2) 3.15A, F250V (P/N 38904) (P/N 38902) Ground The 3-prong power cord plug supplies the ground. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 22: Installing The Turbovap 96

    Connect the other end to the barbed fitting on the Coupling Insert and tighten the clamp. Snap the Coupling Insert (O-ring end) into the Quick-disconnect Gas Inlet on the back of the TurboVap 96. Turn on the gas supply. Release Button 3/8”...
  • Page 23: Install The Venting Hose

    80 psi (5.52 bars) maximum supply pressure. Install the Venting Hose If the TurboVap 96 is not placed under a hood, install the venting hose using the following procedure. Slide one end of the venting hose over the exhaust port.
  • Page 24: Connect The Power Cord

    Turn On the Power To turn on the TurboVap 96, turn ON the power switch located on the lower left side of the unit. When the power is turned on, the internal air temperature will heat up to the previously set plate temperature if it was set to below 37°C;...
  • Page 25: Determining Optimal Concentration Conditions

    > 37C, workstation Cover system runs at … system runs at … Turned on and Either open or Set temperature 37C initialized. closed Evaporation has Closed Set temperature Set temperature started P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 26: Considerations When Setting The Gas Flow Rate

    80 psi (5.52 bars); 60 – 70 psi (4.1 – 4.8 bars) is recommended. WARNING • To avoid injury to yourself or damage to the instrument, DO NOT exceed 80 psi (5.52 bars) maximum supply pressure. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 27: Operation

    Operation Operation This section describes how to operate the TurboVap 96. For each of the two positions, you can choose: • Evaporation time from 1 to 99 minutes, or until stopped manually. • Plate temperature from 20 (ambient) to 80C.
  • Page 28: Setting The Plate Temperature For Position 1

    The flow rate is the total flow for the 96 nozzles in Position 1; it is not a per-nozzle flow rate. Change the flow rate by adjusting the gas regulator knobs on the sides of the TurboVap 96. To set the Flow Rate for position 1: Press the Select button until the Flow Rate light for Position 1 is lit.
  • Page 29: Setting The Gas Time (Evaporation Time) For Position 2

    Press the Select button until the Plate Temp light for position 2 is lit. The display shows the previous set temperature for position 2. Press the up ( ) or down ( ) arrow buttons to display the desired plate temperature. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 30: Setting The Flow Rate For Position 2

    The flow rate is the total flow for the 96 nozzles in Position 2; it is not a per-nozzle flow rate. You change the flow rate by adjusting the gas regulator knobs on the sides of the TurboVap 96, not by changing the setting on the display.
  • Page 31: Starting The Concentration

    Be sure to pull the knob out before making any adjustments to the setting. NOTE The Gas Time and Plate Temperature cannot be changed once the concentration has started. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 32: Elapsed Time Display

    Gas Time for Position 2, and the Position 2 – Gas Time LED will light. (The up, down, and Set buttons have no effect when Cycle Readout is selected.) P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 33: Pausing The Concentration

    37°C; or it will go to 37°C if it is set above this value. • If you set the gas time to 00, you must manually stop the concentration using the Start  Stop button. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 34: Maintenance

    Keep cover clean and do not use the cover as a shelf. Gas Supply Periodically check gas hose and fittings for leaks. Exhaust Port Periodically check for leaks in hose. Replace if necessary. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 35: Replacing The Fuses

    Remove the fuse from the fuse holder and replace it with one of the same type and rating. Replace the fuse holder(s) in the power entry port. Plug in the power cord and turn on the power. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 36: Long Term Storage

    Turn the unit off and unplug the power cord. Remove plates. Turn off and disconnect the air/gas supply. Close the cover. Cover the unit to prevent dirt or dust accumulation. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 37: Troubleshooting

    Troubleshooting Troubleshooting This section provides charts for troubleshooting your concentrator. If the solution listed in the chart is to contact Biotage Technical Support, see “Contact Biotage 1-Point Support” on page Troubleshooting the Concentration To diagnose problems related to the concentration process, locate the description of the condition in the table below.
  • Page 38: Troubleshooting The Front Panel Display

    Problem with flow Contact Biotage (see page sensor. Elapsed Time displays The position has been Restart the position. “--” in Cycle Readout stopped or is not mode. started. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 39: Workstation Not Operational

    Faulty fuse(s). Replace the fuse(s). Faulty control board. Contact Biotage (see page Flow Rate is not Bad sensor PCB. Contact Biotage (see page operational or not correct. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 40: Specifications

    Line Frequency 50 - 60 Hz Fuse 100/120 VAC: (1) 6A, F250V (P/N 38904) 220/240 VAC: (2) 3.15A, F250V (P/N 38902) Time Range 1 to 99 minutes with a one-second resolution. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 41 2 in. (5.1 cm) outside diameter. Vent hose is supplied. Vent hose 2 in. (5.1 cm) inside diameter (supplied) WARNING The exhaust duct MUST be routed to a suitable ventilation system vented outside the laboratory. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 42 Specifications Noise Level The workstation uses an internal exhaust blower. Refer to the Declaration of Conformity for noise level test result. P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 43: Index

    ....37 display during operation ..32 P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 44 ....12 display..... 32 P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 45 ......10 Weight ..... . . 40 P/N 128097 Rev. 00 TurboVap 96 User’s Manual Biotage AB...
  • Page 46 Biotage, AB 10430 Harris Oaks Blvd, Suite C Charlotte, NC 28269 TEL +1 704 654 4900 Toll Free +1 800 446 4752 FAX +1 704 654 4917 http://www.biotage.com...

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