Metrohm 872 IC Pump Manual
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Metrohm 872 IC Pump Manual

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872 Extension Module
IC Pump – 2.872.0010
Manual
8.872.8005EN

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Summary of Contents for Metrohm 872 IC Pump

  • Page 1 872 Extension Module IC Pump – 2.872.0010 Manual 8.872.8005EN...
  • Page 3 Metrohm AG CH-9101 Herisau Switzerland Phone +41 71 353 85 85 Fax +41 71 353 89 01 info@metrohm.com www.metrohm.com 872 Extension Module IC Pump – 2.872.0010 Manual 8.872.8005EN 08.2009 zst...
  • Page 4 Teachware Metrohm AG CH-9101 Herisau teachware@metrohm.com This documentation is protected by copyright. All rights reserved. Although all the information given in this documentation has been checked with great care, errors cannot be entirely excluded. Should you notice any mistakes please send us your comments using the address given above.

  • Page 5: Table Of Contents

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents Table of contents 1 Introduction Instrument description ............1 About the documentation ........... 2 1.2.1 Content and scope ..............2 1.2.2 Symbols and conventions ............2 Safety instructions ..............3 1.3.1 General notes on safety ............3 1.3.2 Electrical safety ................
  • Page 6 Protection ................40 6.4.2 Maintenance ................. 41 Inline filter ................51 6.5.1 Maintenance ................. 51 Quality Management and validation with Metrohm ..53 7 Troubleshooting Problems and their solutions ..........54 8 Technical specifications Reference conditions ............56 Instrument ................56 Ambient conditions ............
  • Page 7 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of contents 10 Accessories 10.1 Scope of delivery ..............63 10.2 Optional accessories ............68 Index ￭￭￭￭￭￭￭￭ 872 Extension Module IC Pump...
  • Page 8 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Table of figures Table of figures Figure 1 Front 872 Extension Module IC Pump ..........6 Figure 2 Rear 872 Extension Module IC Pump ..........7 Figure 3 Setup versions ................... 9 Figure 4 Dismounting the bottle holder ............10 Figure 5 Mounting the bottle holder .............

  • Page 9: Introduction

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction 1 Introduction Instrument description Existing 850 Professional IC instruments can be expanded to include addi- tional functions by means of 872 Extension Modules. Every 850 Professio- nal IC instrument can be supplemented with up to 3 extension modules. The 872 Extension Module –...

  • Page 10: About The Documentation

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.2 About the documentation Pulsation damper The pulsation damper protects the separation column from damage caused by pressure fluctuations when switching the injection valve, and reduces interfering pulsations during highly sensitive measurements. About the documentation Caution Please read through this documentation carefully before putting the instrument into operation.

  • Page 11: Safety Instructions

    The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010. Warning Only personnel qualified by Metrohm are authorized to carry out service work on electronic components. ￭￭￭￭￭￭￭￭ 872 Extension Module IC Pump...

  • Page 12: Tubing And Capillary Connections

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1.3 Safety instructions Warning Never open the housing of the instrument. The instrument could be damaged by this. There is also a risk of serious injury if live components are touched. There are no parts inside the housing which can be serviced or replaced by the user.

  • Page 13: Flammable Solvents And Chemicals

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 1 Introduction 1.3.4 Flammable solvents and chemicals Warning All relevant safety measures are to be observed when working with flammable solvents and chemicals. Set up the instrument in a well-ventilated location (e.g. laboratory ￭ flue). Keep all sources of flame far from the workplace. ￭...

  • Page 14: Overview Of The Instrument

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2.1 Front 2 Overview of the instrument Front Figure 1 Front 872 Extension Module IC Pump Eluent degasser Coupling 6.2744.230 See Chapter 4.5 For connecting the eluent aspiration tubing. High pressure pump Purge valve See Chapter 4.6 See Chapter 4.6 Inline filter Pulsation damper See Chapter 4.7...

  • Page 15: Rear

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 2 Overview of the instrument Rear to Vacuum Transport security screws Made by Metrohm Herisau Switzerland Figure 2 Rear 872 Extension Module IC Pump Transport locking screws Connector In To connect the extension module to the IC instrument or to a previous extension mod- ule.

  • Page 16: Assembly

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.1 General 3 Assembly General The extension modules are fitted directly to the 850 Professional IC instru- ment and connected with it via 6.2156.060 connection cable. Extension modules have no power supply of their own, but rather draw the electric- ity they require from the instrument with which they are connected.

  • Page 17: Mounting The Extension Module Onto The Ic Instru- Ment

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Assembly Figure 3 Setup versions Extension module above the IC instru- Extension module on the below the IC ment instrument Between the 850 Professional IC and the Between the base plate and the 850 Profes- bottle holder. sion IC. Extension module next to the IC instru- ment With its own base plate and its own bottle...

  • Page 18: Figure 4 Dismounting The Bottle Holder

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.2 Mounting the extension module onto the IC instrument 4 Dismounting the bottle holder Figure 4 Dismounting the bottle holder Cover stoppers Cylinder screws Remove covering stoppers (4-1). ￭ Loosen the cylinder screws with a 6.2621.100 3 mm hexagon ￭...

  • Page 19: Figure 5 Mounting The Bottle Holder

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Assembly 6 Mounting the bottle holder Figure 5 Mounting the bottle holder Cover stoppers Cylinder screws Attach the bottle holder on the extension module. ￭ Tighten the cylinder screws (4-2) with an 6.2621.100 3 mm hexa- ￭ gon key Insert covering stoppers (4-1).

  • Page 20: Mounting The Extension Module Below The Ic Instru- Ment

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.3 Mounting the extension module below the IC instrument 9 Mounting the drainage tubing Reconnect the drainage tubing to the drainage tubing connector of the bottle holder. Possibly, a longer section of silicone tubing 6.186.020 must be cut to fit and mounted (see also the manual for the IC instrument).

  • Page 21: Figure 6 Removing The Base Tray

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Assembly Figure 6 Removing the base tray Base tray Cylinder screws With washer. 6 Mounting the base tray Tilt the extension module sideways and lay it down flat. ￭ Attach base tray. ￭ Slide the washers onto the cylinder screws (7-2) and tighten these ￭...

  • Page 22: Figure 7 Mounting The Base Tray

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.3 Mounting the extension module below the IC instrument Figure 7 Mounting the base tray Base tray Cylinder screws With washer. Set up the extension module. ￭ Optional: Set up further extension modules. ￭ Set up the IC instrument. ￭...

  • Page 23: Setting Up The Extension Module Next To The Ic Instrument

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Assembly 9 Inserting the detector(s) again and connecting it (them) See manual for the IC instrument. 10 Restoring the loosened connections Reconnect the drainage tubings, ￭ Possibly, a longer section of silicone tubing 6.186.020 must be cut to fit and mounted (see also the manual for the IC instru- ment).

  • Page 24: Figure 8 Mounting The Base Tray

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.4 Setting up the extension module next to the IC instrument Figure 8 Mounting the base tray Base tray Cylinder screws With washer. Set up the extension module. ￭ Optional: Set up further extension modules. ￭ ￭￭￭￭￭￭￭￭ 872 Extension Module IC Pump...

  • Page 25: Figure 9 Mounting The Bottle Holder

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Assembly 3 Mounting the bottle holder Figure 9 Mounting the bottle holder Cover stoppers Cylinder screws Place the bottle holder on the extension module. ￭ Tighten the cylinder screws (9-2) with an 6.2621.100 3 mm hexa- ￭ gon key. Insert covering stoppers (9-1).

  • Page 26: Figure 10 Connecting The Drainage Tubings

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.4 Setting up the extension module next to the IC instrument 6 Connecting the leak sensor Plug the 6.2103.170 adapter into the leak sensor connector of ￭ the IC instrument. Connect the leak sensor cable of the IC instrument to the adapter. ￭...

  • Page 27: Connecting The Vacuum Pump(S)

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Assembly Drainage tubing connection Drainage tubing connector For supplying escaped liquid through the For draining escaped liquid from the base connected drainage tubing to the leak sen- tray through the connected drainage tubing. sor. Drainage tubing Section of the 6.1816.020 silicon tubing. Guides escaped liquid into a waste con- tainer.

  • Page 28: Figure 11 Connecting The Vacuum Pump

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3.5 Connecting the vacuum pump(s) “to Vacuum” 872 Extension Module 1 “to Vacuum” 872 Extension Module 2 “Vacuum” 850 Professional IC Figure 11 Connecting the vacuum pump T connector 6.1808.060 FEP tubing 6.1805.050 For connecting several FEP tubings. Connect to the connector to Vacuum on the first 872 Extension Module.

  • Page 29: Installation

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation 4 Installation About this chapter The Installation chapter contains this overview ￭ a brief set of instructions for the installation of the 872 Extension Mod- ￭ ule IC Pump (see Chapter 4.2, page 21). At each step you will find cross-references to detailed installation instructions for individual com- ponents, should you require such aids.

  • Page 30: Installation Diagram

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.3 Installation diagram Connect the other end of the 6.1831.100 connection capillary ￭ (12-2)/(13-2) either with – a 6.2744.070 pressure screw to the T distributor (12-7) of the gradient mixing coil (gradient system) – a 6.2744.014 pressure screw to the injection valve of the 850 Professional IC instrument (isocratic system).

  • Page 31: Figure 12 Installation Diagram - Gradient

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation High pressure gradi- ent system Figure 12 Installation diagram – gradient Eluent aspiration tubing 6.1834.080 Connection capillary 6.1831.100 Connection eluent bottle – eluent degasser Connection pulsation damper – gradient mixing coil PEEK pressure screw, short 6.2744.070 Connection capillary 6.1831.100 Connection to another high pressure pump Gradient mixing coil 6.2758.000 PEEK pressure screw 6.2744.010...

  • Page 32: Eluent

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.4 Eluent Isocratic system Figure 13 Installation diagram – isocratic Eluent aspiration tubing 6.1834.080 Connection capillary 6.1831.100 Connection eluent bottle – eluent degasser Connection pulsation damper – IC instru- ment PEEK pressure screw, short 6.2744.070 The following chapters describe the individual installation steps in detail. Eluent 4.4.1 Connecting eluent bottle...

  • Page 33: Figure 14 Installing Eluent Bottle Attachment

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation Assembling eluent aspiration tubing 1 Guide the free end of the eluent aspiration tubing (14-1) out of the instrument through a suitable capillary feed-through. 2 Installing the 6.1602.160 eluent bottle attachment Slide tubing nipple (14-2) and O-ring (14-3) onto the eluent aspi- ￭...

  • Page 34: Figure 16 Installing Tubing Weighting And Aspiration Filter

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.4 Eluent 4 Installing tubing weighting and aspiration filter Figure 16 Installing tubing weighting and aspiration filter Eluent aspiration tubing 6.1834.080 Eluent bottle attachment 6.1602.160 Tubing weighting Clamping screw From accessory set 6.2744.210. From accessory set 6.2744.210. Aspiration filter 6.2821.090 With filter holder from accessory set 6.2744.210.

  • Page 35: Figure 18 Eluent Bottle - Connected

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation Fasten the bottle attachment (16-2) on the eluent bottle (18-10). ￭ The aspiration filter (18-6) must rest on the base of the eluent bottle. 6 Mounting the adsorber tube Note In the case of alkaline eluents and eluents with lower buffer capacity, the eluent bottle must be equipped with a CO adsorber (18-4).

  • Page 36: Eluent Degasser

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.5 Eluent degasser Eluent Aspiration filter 6.2821.090 Filter holder Clamping screw From accessory set 6.2744.210. From accessory set 6.2744.210. Tubing weighting 10 Eluent bottle 6.1608.070 From accessory set 6.2744.210. 11 Bottle attachment 6.1602.160 12 SGJ clip 6.2023.020 13 Tubing nipple 14 Thread stopper Eluent degasser Gas bubbles in the eluent lead to an unstable baseline, as high pressure...

  • Page 37: High Pressure Pump

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation Tubing flare Clamping screw With tubing nipple. Eluent aspiration tubing 6.1834.080 Connection capillary 6.1834.090 For aspirating the eluent. The clamping Connection from the eluent degasser to the high pressure pump (see Chapter 4.6, page screw (19- ) is firmly mounted. 29).

  • Page 38: Figure 20 Capillary Connections High Pressure Pump/Purge Valve

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.6 High pressure pump Figure 20 Capillary connections high pressure pump/purge valve Connection capillary PEEK pressure screw, short 6.2744.070 PEEK capillary, connects main piston and auxiliary piston. Outlet valve holder Pump head 6.2824.110 Fastening screws Inlet valve holder For fastening the pump head. Pump head input capillary Pressure screw PEEK capillary at the input of the pump...

  • Page 39: Figure 21 High Pressure Pump - Connect Inlet

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation Note The eluent aspiration tubing is already installed in the newly delivered instrument. The following installation instructions need not be carried out at the time of initial installation. Connecting inlet to the high pressure pump Figure 21 High pressure pump –...

  • Page 40: Deaerating The High Pressure Pump

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.6 High pressure pump 4.6.2 Deaerating the high pressure pump The high pressure pump will only operate perfectly if the pump head con- tains no more air bubbles. Therefore it must be deaerated during initial start-up and after every change of eluent. Caution The high pressure pump must not be deaerated before the initial start- up .

  • Page 41: Figure 22 Deaerating The High Pressure Pump

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation Deaerating the high pressure pump The instrument must be connected to the PC and switched on to deaerate the high pressure pump. Figure 22 Deaerating the high pressure pump Syringe 10 mL 6.2816.020 Luer connector For aspirating the eluent. On purging needle.

  • Page 42: Inline Filter

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.7 Inline filter 4 Setting the flow rate Start MagIC Net (if not yet started). ￭ Ensure that the eluent aspiration tubing is immersed sufficiently in ￭ the eluent. Let the high pressure pump run. ￭ 5 Aspirating eluent Aspirate with the syringe (22-1) until bubble-free eluent flows into ￭...

  • Page 43: Pulsation Damper

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4 Installation Installing the inline filter Caution Observe the flow direction marked on the filter housing for the connec- tion of the inline filter. Figure 23 Connecting inline filter Connection capillary PEEK pressure screws, short Connects the purge valve with the inline fil- 6.2744.070 Inline filter 6.2821.120 Connection capillary...

  • Page 44: Figure 24 Pulsation Damper - Connection

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 4.8 Pulsation damper The pulsation damper protects the separation column from damage caused by pressure fluctuations when switching the injection valve, and reduces interfering pulsations during highly sensitive measurements. In order to ensure these functionalities, it must be connected between the high pressure pump (see Chapter 4.6, page 29) and injection valve .

  • Page 45: Start-Up

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 5 Start-up 5 Start-up The extension module is put into operation together with the IC instru- ment. Putting IC instrument into operation with extension mod- ules 1 Start MagIC Net. 2 Connect IC instrument to PC and switch on. The extension module is recognized automatically by MagIC Net.

  • Page 46: Operation And Maintenance

    Metrohm. If working frequently with caustic and corrosive chemicals, a shorter mainte- nance interval is recommended. The Metrohm service department offers every form of technical advice for maintenance and service of all Metrohm instruments. 6.1.3...

  • Page 47: Shutting Down

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Operation and maintenance 6.1.4 Shutting down If the instrument is shut down for a longer period of time, the entire IC system must be rinsed as follows to rid it of salts in order to prevent elu- ent salts from forming crystals which may cause subsequent damage. rinse all capillaries and the Dosino with methanol/ultra pure water ￭...

  • Page 48: Operation

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.4 High pressure pump pH changes result in shifts in the dissociation equilibria and hence changes in the retention times. Organic solvents The addition of an organic solvent (e.g. metha- nol, acetone, acetonitrile) to aqueous eluents generally accelerates lipophilic ions. 6.3.2 Operation 6.3.2.1...

  • Page 49: Maintenance

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Operation and maintenance Salt crystals between the piston and seal cause abrasion particles which can find their way into the eluent. These lead to contaminated valves, a rise in pressure and in extreme cases scratched pistons. It is therefore essential to ensure that no precipitates can occur (see Chapter 6.3.2.3, page 40).

  • Page 50: Figure 25 Removing Piston

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.4 High pressure pump piston is on the left (viewed from the front), and the auxiliary piston is on the right. Cleaning/replacing the zirconium oxide piston Clean one piston after the other as follows: 1 Removing the piston cartridge from the pump head Loosen the piston cartridge with a wrench and unscrew from the pump head by hand.

  • Page 51: Figure 26 Components Of The Piston Cartridge

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Operation and maintenance Remove the spring retainer, spring and the inner plastic sleeve ￭ from the piston cartridge and lay by. Remove the backup ring from the pump head and lay to the other ￭ parts. Figure 26 Components of the piston cartridge Piston cartridge screw Retaining washer...

  • Page 52: Figure 27 Tool For Piston Seal 6.2617.010

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.4 High pressure pump Replacing the piston seal The 6.2617.010 special tool (see Figure 27, page 44) is necessary in order to remove the piston seal from the pump head. It consists of two parts: a tip for removing the old piston seal and a sleeve for inserting the new piston seal.

  • Page 53: Figure 28 Removing The Piston Seal

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Operation and maintenance Figure 28 Removing the piston seal Piston seal Tool for piston seal Pin of the tool. 2 Inserting the new piston seal into the tool Insert the new piston seal tightly by hand into the recess of the sleeve of the tool for the piston seal (27-2).

  • Page 54: Figure 30 Inserting The Piston Seal Into The Pump Head

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.4 High pressure pump Figure 30 Inserting the piston seal into the pump head 4 Replacing the piston cartridge Screw the assembled piston cartridge back into the pump head and tighten, first by hand, then additionally by approx. 15° with a wrench.

  • Page 55: Figure 31 Removing Valves

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Operation and maintenance Figure 31 Removing valves Outlet valve holder Outlet valve Order number: 6.2824.160 Inlet valve Inlet valve holder Order number: 6.2824.170 2 Cleaning undissected valve Clean contaminated or blocked valves initially without dismantling them completely. Rinse the valve in eluent flow and counterflow direction using a ￭...

  • Page 56: Figure 32 Dismantling Valve

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.4 High pressure pump Place the valve with the seal faced downwards above the recess ￭ in the holder. Push the valve components out of the valve housing using the ￭ needle of the tool. Figure 32 Dismantling valve Needle Valve For pushing the valve components out of...

  • Page 57: Figure 33 Components Of The Inlet Valve And Outlet Valve

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Operation and maintenance Figure 33 Components of the inlet valve and outlet valve Inlet valve 6.2824.170 Outlet valve 6.2824.160 Inlet valve housing Outlet valve housing Sealing ring (black) Sleeve Sapphire sleeve Ruby ball The shiny side must point to ruby ball. Ceramic holder for ruby ball 10 Seal The larger opening must point outwards.
  • Page 58 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.4 High pressure pump Place the valve housing over the stacked components and hold it ￭ tightly. By tilting the tool, the valve components slide into the valve hous- ￭ ing. Press the seal by hand well on the valve housing. ￭...

  • Page 59: Inline Filter

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6 Operation and maintenance Mounting the pump head Note To prevent the pump head from being positioned the wrong way, it is provided with different bore hole depths for the fastening bolts, i. e. a fastening bolt is longer than all others. The bore hole with the greatest depth must therefore be assigned to the longest bolt.
  • Page 60 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 6.5 Inline filter Changing the filter The flow must be stopped before changing the filter. 1 Removing the inline filter Unscrew the pressure screws (34-1) from the inline filter. ￭ 2 Unscrewing the filter screw Screw the filter screw (34-4) out of the filter housing (34-2) with ￭...

  • Page 61: Quality Management And Validation With Metrohm

    Metrohm» available from your local Metrohm agent. Validation Please contact your local Metrohm agent for support in validating instru- ments and software. Here you can also obtain validation documentation to provide help for carrying out the Installation Qualification (IQ) and the Operational Qualification (OQ).

  • Page 62: Troubleshooting

    Check connections of the eluent degasser (see to the retention eluent. Chapter 4.5, page 28). times in the chroma- High pressure pump – Request Metrohm Service. tograms defective. Vacuum is not being Eluent Degasser – Connec- Seal the connector Vacuum tightly with a ￭...
  • Page 63 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 7 Troubleshooting Problem Cause Remedy Connect an FEP tubing between the IC ￭ instrument and the Extension Module and tighten both clamping screws until they seal. ￭￭￭￭￭￭￭￭ 872 Extension Module IC Pump...

  • Page 64: Technical Specifications

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8.1 Reference conditions 8 Technical specifications Reference conditions The technical specifications listed in this chapter refers to the following reference conditions: Ambient tempera- +25 °C (±3 °C) ture Instrument status > 40 minutes in operation (equilibrated) Instrument IC system Metal-free IC system Painted polyurethane hard foam without CFCs, fire class V0 Material...

  • Page 65: Housing

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8 Technical specifications Housing Dimensions Width 365 mm Height 131 mm Depth 380 mm Material of base Polyurethane hard foam (PUR) with flame retardation for fire class tray, housing and UL94V0, CFC-free, coated bottle holder Eluent degasser Material fluoropolymer Resistance to sol- No restriction (apart from PFC) vents...

  • Page 66: Interfaces

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8.7 Interfaces Safety shutdown Function Automatic shutdown upon reaching the pressure limit values Maximum pres- Adjustable from 0.1…50 MPa (1…500 bar) ￭ sure limit The pump is automatically shut down at the first piston stroke ￭ above the maximum limit value Minimum pres- Adjustable from 0…49 MPa (0…490 bar) ￭...

  • Page 67: Weight

    ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 8 Technical specifications 8.10 Weight 1.872.0010 7.7 kg (without accessories) ￭￭￭￭￭￭￭￭ 872 Extension Module IC Pump...

  • Page 68: Conformity And Warranty

    Manufacturer Metrohm Ltd., CH-9101 Herisau/Switzerland Metrohm Ltd. is holder of the SQS certificate ISO 9001:2000 Quality man- agement system for development, production and sales of instruments and accessories for ion analysis. Herisau, 31 March, 2008 ￭￭￭￭￭￭￭￭...

  • Page 69: Quality Management Principles

    Components All components used in the Metrohm instruments have to satisfy the qual- ity standards that are defined and implemented for our products. Suppli- ers of components are audited by Metrohm as the need arises.

  • Page 70: Warranty (Guarantee)

    Warranty (guarantee) Metrohm guarantees that the deliveries and services it provides are free from material, design or manufacturing errors. The warranty period is 36 months from the day of delivery; for day and night operation it is 18 months.
  • Page 71 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10 Accessories 10 Accessories Note Subject to change without notice. 10.1 Scope of delivery 2.872.0010 872 Extension Module – IC Pump Qty. Order no. Description 1.872.0010 872 Extension Module – IC Pump 6.1602.160 Eluent bottle attachment GL 45 For eluent bottles; with connections for adsorber tube and aspiration tubing.
  • Page 72 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10.1 Scope of delivery Qty. Order no. Description 6.1609.000 Adsorber tube / large and bent For filling with adsorber material. Material: Glass Height (mm): Inner diameter (mm): SGJ size: B-14/15 6.1805.060 FEP tubing / M6 / 60 cm Protected against light and kink. Material: Inner diameter (mm): Length (mm):...
  • Page 73 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10 Accessories Qty. Order no. Description 6.1834.080 Aspiration tubing, 2 m Aspiration tubing for Professional IC instruments Material: PTFE Outer diameter (mm): Inner diameter (mm): Length (m): 6.2023.020 Clip for SGJ 14/15 Clip for SGJ 14/15 Material: 6.2156.060 Cable extension module - Professional IC, 40 cm Cable for the connection of an extension module to a Professional IC instrument...
  • Page 74 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10.1 Scope of delivery Qty. Order no. Description 6.2744.070 Pressure screw short Short version. With UNF 10/32 connection. 5 pieces. For the connec- tion of PEEK capillaries Material: PEEK Length (mm): 6.2744.210 Tubing adapter for aspiration filter For Professional IC instruments 6.2758.000 Mixing coil for high presssure gradients For mixing high pressure gradients...
  • Page 75 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10 Accessories Qty. Order no. Description 6.2816.040 Purging needle With PTFE tubing and Luer connection. For syringes. For aspirating eluents. 6.2821.090 Aspiration filter Pore size 20 µm. Set of 5 pieces. For 6.1834.000 aspiration tubing and 6.1821.040 and 6.1821.050 filter tubes. Material: Outer diameter (mm): Length (mm):...
  • Page 76 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10.2 Optional accessories 10.2 Optional accessories 2.872.0010 872 Extension Module – IC Pump Order no. Description 6.2061.100 Flask holder (ProfIC) Flask holder for Professional IC instruments 6.2061.110 Base tray with sensor for Professional IC systems 6.2103.170 Adapter for leak sensor in Professional IC Adapter for the connection of two leak sensors to one Professional IC instru- ment 6.2156.070...
  • Page 77 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 10 Accessories Order no. Description 6.2744.240 Cross connection UNF 10-32 PEEK Mixing connection for three solutions 6.2824.130 Macro pump head PEEK Macro pump head for intelligent IC instruments, flow range 0.1...20 mL/min, maximum pressure 12.5 MPa. Material: PEEK (metal-free) 6.5332.000 IC tubing set for a second extension module 6.9988.503...
  • Page 78 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Index Index Numbers/Symbols Eluent degasser Maintenance 6.2821.090 aspiration filter ..40 Installation ......28 High pressure pump ... 40 6.2821.130 filter ...... 51 Technical specifications ..57 Pump head ......41 Material ........57 Accessories Filter Optional ......68 see also "inline filter"...
  • Page 79 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ Index Temperature ......56 Validation ......... 53 Warranty ........62 Transport ......... 56 Valves of the high pressure pump ..........49 Vacuum pump ......19 ￭￭￭￭￭￭￭￭ 872 Extension Module IC Pump...

This manual is also suitable for:

2.872.0010

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