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Tamson Instruments TV2000 AKV Manual

Automated kinematic viscosity
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Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands .
\\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK
MANUAL
TV2000 AKV
Automated
Kinematic
Viscosity
+31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41
page 1 / 60

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Summary of Contents for Tamson Instruments TV2000 AKV

  • Page 1 MANUAL TV2000 AKV Automated Kinematic Viscosity Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 1 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 2: Safety And Warnings

    Make sure you read and understand all instructions and safety precautions listed in this manual, before installing or operating the equipment. If there are any questions concerning the operation of the equipment or about the information in this manual please contact your local dealer or Tamson Instruments sales de- partment first.

  • Page 3: Table Of Contents

    Cleaning of the glass viscometers ....................27 Preparation of the sample ......................... 29 Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 3 / 60...
  • Page 4 Spare parts list measuring head ....................... 60 Spare partlist for fluid trap ........................ 60 DISCLAIMER ......................60 Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 4 / 60...
  • Page 5 ……….…………………………………………………. Name of dealer: ……….…………………………………………………. ………………………………….………………………. Signature: …...……………………… Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 5 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 6: Ec Declaration Of Conformity Thermostatic Bath T-Series

    1 January 1996, Tamson Instruments bv, The Netherlands Ing. R.C. van Hall Director Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 6 / 60...

  • Page 7: Delivery Checklist

    Tube connection(s) Sensitivity (For test result please see the separately added calibration certificate.) Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 7 / 60...

  • Page 8: Precautions And Hazards

    Instead reverse flow tubes should be used. These unfortunately are not available for the AKV system. A sample can always be send to Tamson instruments to make sure the unit can be used for these specific samples.

  • Page 9: Safety Systems

    ’errors’. In this way there is a continual check of the proper functioning of the bath. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 9 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 10: Installation

    Installation Important TAMSON INSTRUMENTS b.v. is not responsible in any way for consequential damage or harm caused by using this bath. Whilst cleaning, servicing or repairing always disconnect the bath from the mains (by unplugging the power cord). Well-trained and authorized persons may only carry out repairs on the electrical system of the bath.
  • Page 11 Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 11 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.
  • Page 12 Figure 1 Cooling apparatus TLC10 and TLC15 MOTOR FUSE Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 12 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 13: Operating The Bath

    Changing the password can be done by selecting ”Enter security code” again. Entering ”0” will disable the password function. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 13 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 14: Adjusting Set Point

    Therefore it is advisable to Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 14 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 15: Setting Power Limit

    LCD-display is that the contrast of the display defines the viewing angle under which the display can be Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 15 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 16: Backlight

    Backlight with the “MODE” key. Using the ”UP” and ”DOWN” keys to adapt the intensity of the backlight in 16 steps (0 .. 15). Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 16 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 17: Akv (Viscometer) Manual

    START, E or MODE bath. A vacuum set too strong will result in a fountain Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 17 / 60...

  • Page 18: The Akv Menu Structure

    The cursor is blinking on the first figure. Enter a numer- ical value of max. 4 digits. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 18 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 19: Store New Viscometer Parameters

    Writing table After completion of this operation the display automati- cally returns. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 19 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 20: Delete A Viscometer From Memory

    “SELECT VISCOMETER” Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 20 / 60...

  • Page 21: Entering A Sample Number

    The “s” behind the viscometer number indicates the currently selected viscometer. After the printout is completed return by pressing the “Start/Stop” key. Setting a pre-heating time Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 21 / 60...

  • Page 22: Setting The Tube Vacuum

    The vacuum can be adjusted by turning the screw of Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 22 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 23: Enter Number Of Runs

    When a sample is very light or the START, E or MODE Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 23 / 60...

  • Page 24: Adjusting Backlight

    Now press the “LF” key several Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 24 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 25: Rs232 Communication

    RS232 of the TV2000 bath is not available for control or read out of parameters i.e. like PV, SP etc. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 25 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 26: Preparation For Measurement

    Fluctuating, deviating Keep tubes used for silicone sample separated Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 26 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 27: The Type Of Viscometer Tube

    It can damage the viscometer tube or cause accidents when solvent is sprayed around. Always wear protective clothing (gloves, eye protection etc.). Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 27 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.
  • Page 28 Use warm dry air or nitrogen to remove any remains of the cleaning solvent or moisture. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 28 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 29: Preparation Of The Sample

    Make sure sample is at least at the same temperature or warmer than ambient and glass viscometer, Do not pour sample from the viscometer tube back into sample container(B). Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 29 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 30: Charging The Viscometer Tube

    When pre-heating, prevent gas from building up pressure in the sample container. use open fire(A) or hot plate(B) to pre-heat sample Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 30 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.
  • Page 31 Mount new tip for next sample. Upper filling mark Lower filling mark Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 31 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 32: Measurement

    Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 32 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...
  • Page 33 Result is calculated Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 33 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 34: Connecting Glass Viscometer Tube And Measuring Head

    (4) is blue. Fig. 2 Connecting tubes measuring head (Top view) Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 34 / 60...

  • Page 35: Fluid Trap

    Top view Front view (Measuring head not attached) Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 35 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 36: Adjustment Of The Akv-System Before Performing A Run

    Press “Start/Stop” key again and repeat the above described procedure. Fig. 4 Backside of TV2000 AKV Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 36 / 60...

  • Page 37: Start A Single Run

    Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 37 / 60...
  • Page 38 Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 38 / 60...
  • Page 39 1 minute and after than the vacuum devices are switched-on again to draw the sample up into the measuring capillary. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 39 / 60...

  • Page 40: Measurement Examples

    445.10 sec Visc: 41,9996 cSt Av, Visc: 41.9974 cSt Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 40 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...
  • Page 41 461.31 sec Visc: 20.2007 cSt Av, Visc: 20.2372 cSt Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 41 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 42: Aborting A Run

    41,9977 cSt *********TEST ABORTED ******** Flow time 10.45 Visc Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 42 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 43: Trouble Shooting

    The power supply is too low and due to that the current detector is unable to operate correctly. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 43 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.
  • Page 44 This error can be reported both on the display as send by RS232 when using the command ER. This error indicates that during the analogous-digital conversion the microprocessor has detected a value, which is out Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 44 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 45: Bath Temperature Does Not Become Stable

    If the operating temperature is far above the ambient temperature it is most likely that the viscosity Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 45 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 46: Problems With Measuring Head: Bad Repeatability

    Bath fluid level too low o Adjust fluid level by filling the bath. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 46 / 60...
  • Page 47 The following two measuring results show the difference between a well performed measurement and a measurement with bad repeatability which is caused by one of problems described above. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 47 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.
  • Page 48 Av, Visc: 04.4811 cSt Av, Visc: 04.4879 cSt Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 48 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 49: Problems With Measuring Head: Bad Detection

    Instead reverse flow tubes should be used. These unfortunately are not availa- ble for the AKV system. A sample can always be sent to Tamson Instruments to make sure the unit can be used for specific samples. If the meniscus can be detected by eye, the AKV system will be able to detect and measure the flow times.

  • Page 50: Akv Display Shows "Visco Not Empty

    If such is the case with the sample, the D445 method and routine flow tubes can not be used to perform methods for these types of samples. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 50 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev.

  • Page 51: Trouble Shooting The Measuring Head

    Press key "3" the IR sensors start to "tune" and after several seconds new reading follows on the display. Note down the reading. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 51 / 60...
  • Page 52 AKV must be checked. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 52 / 60...

  • Page 53: Technical Specifications

    - ASTM reference thermometer - Bath filling - Vacuum pump Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 53 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 54: Specifications Bath (Tv2000)

    - Cooling coil - Leveling feet - Communication port Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 54 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 55: Technical Drawing: Akv Unit

    28T4150 Chassis socket viscometer Green(6) (Seen at backside) Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 55 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 56: Technical Drawing: Thermostatic Bath

    Part numbers mentioned in this drawing refer to 28T4057 230 Volt version Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 56 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 57: Accessories And Spare Parts

    AKV/500 25T0789 AKV/600 on reqest. 4000 - 20000 Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 57 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 58: Indicating Thermometers

    To protect the thermometer for mechanical damage a stainless steel holders is available ordering code 00T0239. Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 58 / 60...

  • Page 59: Spare Parts List Bath

    06T1942 PCB measuring head 24T7937 DIN-connector electronic cable Tamson Instruments bv, van 't Hoffstraat 12, 2665 JL Bleiswijk, Netherlands . +31(0)10 – 522 43 73 Fax. +31(0)10 – 521 19 41 page 59 / 60 \\word\manuals\tv\akv.doc Date 10-2010 Rev. 1.02jUK...

  • Page 60: Spare Parts List Akv-System

    Alteration of this document is strictly prohibited. Except to the extent required by law, republica- tion or retransmission of this document, in whole or in part, is not permitted. Tamson Instruments bv as- sume no responsibility for accuracy of information. Tamson Instruments neither represent nor warrant that the format, content or product formulas contained in this document comply with the laws of any other coun- try except the Netherlands.

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