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USING MANUAL
FIRST PLUS LR
1

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SONIA CASTIGLIONE
February 25, 2025

taratura interna dello strumento

1 comments:
Mr. Anderson
February 25, 2025

The internal calibration process for the Lamy Rheology FIRST PLUS LR involves the following steps:

1. Install the Spindle: Refer to section 3.1 and install spindle L2.
2. Select Spindle and Speed: Go to section 2.2.2, select spindle L2, and set the speed to 60 rpm.
3. Zero Adjustment: Perform a zero adjustment.
4. Immerse the Spindle: Follow section 3.2 to immerse the spindle in the standard oil at the correct level (marked on the spindle).
5. Wait for Temperature Stabilization: Allow 15 minutes for the standard oil to reach the correct temperature.
6. Set Measurement Parameters: Select a measuring time of 60 seconds and start the measurement at 60 rpm.
7. Check the Result: The result should be within ±5% of the standard viscosity value.
8. Troubleshooting: If the measurement is out of range, check for errors such as incorrect filling, zero adjustment, spindle rotation, or temperature settings. If necessary, recalibrate the instrument.

This process ensures accurate and reliable viscosity measurements.

This answer is automatically generated

Summary of Contents for Lamy Rheology FIRST PLUS LR

  • Page 1 USING MANUAL FIRST PLUS LR...
  • Page 2: Table Of Contents

    CONTENTS 1 INTRODUCTION ..........................3 1.1 COMPONENTS ..........................4 1.2 GENERAL VIEW OF YOUR DEVICE ..................5 1.3 CONNEXIONS ..........................7 1.4 SPECIFICATIONS ........................7 1.5 INSTALLATION ........................... 8 2 GETTING STARTED ........................... 9 2.1 STATE ICONS ..........................9 2.2 PRIMARY CONCEPTS ......................10 2.2.1 MAIN MENU ........................10 2.2.2 MEASURE...........................10 2.2.3 VIEW RESULT ........................13...
  • Page 3: Introduction

    1. INTRODUCTION The FIRST PLUS is a device able to measure the viscosity, which is the capacity of a product to resist to the flow. The fluid is forced to a shear rate (rotational speed) and the shear stress (motor torque) is measured.
  • Page 4: Components

    1.1. COMPONENTS Viscometer is delivered inside a foam protection to avoid any problem during transport. According to your order this foam can be inside a box or a carrying case and can contain measuring system. In detail, you will find different part in your box as shown below. Screw and tool Delrin cylinder Aluminium Arm...
  • Page 5: General View Of Your Device

     On / Off Switch Always with the aim of improving your experience, LAMY RHEOLOGY has decided to equip all of its PLUS range with a luminous and design switch. It has been placed in the centre of the device for greater intuitiveness.
  • Page 6  Aluminium arm The aluminium arm is equipped with the clamping knob allows you to maintain the height of the measuring head and a handle for easy handling. The measuring head is fixed to the arm by one screw. Screw to keep measuring head in higher position Handle for manipulation Screw to fix the measuring...
  • Page 7: Connexions

    1.3. CONNEXIONS According to your order, rear panel of device get this available connexions. Connection for Pt100-2 probe or 4-20mA output Connection mini USB for PC control Connection for USB stick or printer Network Connection Ethernet for service Serial Connection for PC control Connection for power câble 1.4.
  • Page 8: Installation

    1.5. INSTALLATION Your viscometer should be installed in a clean, vibration-free environment. Even if no level is necessary, choose a stable and flat table. This installation notice concern only viscometer without any temperature device. If you have it, please refer to specific notice of temperature unit for installation. After unpacking all accessories from the box (or case if it is supplied), you must first screw the rod to the base with screw and key provided.
  • Page 9: Getting Started

    Your viscometer will be used with different measuring system. To know how to mount and use it, please refer section 3. 2. GETTING STARTED Once power cable has been plugged on rear panel of device (see section 1.3), you can click on button to switch on your device (see section 1.2).
  • Page 10: Primary Concepts

    Software remote control 2.2.2. Measure Measure tab is central part of your FIRST PLUS LR. Before to use it, you should install your measuring system and your sample. Please see section 3. Then you click on “Measure”, you will see a new window.
  • Page 11 Manual Mode enables to choose your measurement parameters like «Measuring System », « Speed or shear rate» then « Time of measurement ». Select your measuring system Choose speed or shear rate Choose time for measurement (minimum 10 s) Rq : If « Time » = 0, you could modify « speed » during the measurement. This could help you to define the best conditions to work on your sample.
  • Page 12 Then you can click “Start” to start your measurement. While your measurement, you will see a torque gage. Please try to not be closed to the upper and lower limit. Please increase speed or take a bigger measuring system if you are close to the lower limit. Please decrease speed or choose smaller measuring system if torque reading is close to the upper limit.
  • Page 13: View Result

    By click on tab “List of measurement data” you could see all saved measurement made with your FIRST PLUS LR. You could select which one you want to read. Then you selected a measure, you will see result and get possibility to print it if a printer is connected.
  • Page 14: Remote Control

    "File", "Open", taking care to select "All files *. *". Excel will offer you to convert your data by displaying three successive windows. Be careful not to change the options offered except on the second where it will be necessary to choose the option "semicolon" for the separation of the columns.
  • Page 15: Parameters

    This icon is only available then you are in “Main menu”. 2.2.5.1. Languages Enable you to select language of your FIRST PLUS LR. You have choice between French, English, Russian and Spanish. Then you have selected your desired language, you have to click on “Ok”...
  • Page 16: Date / Hour

    2.2.5.2. Date / Hour Enable you to adjust hour and date of your FIRST PLUS LR. 2.2.5.3. Sounds/Standby/Lighting Allow you to modify sounds, lighting and activate or not the Standby mode of your FIRST PLUS Choose if you want to get sound during using touch screen.
  • Page 17: User Name

    2.2.5.4. User Name Operator mode will allow you to create different operators for your FIRST PLUS LR. The use of the operators makes it possible to identify the person making the measurement. Operator management must always begin with the creation of the first account, which will become the administrator and thus create or delete another operator account.
  • Page 18 To use the operator accounts you must activate the mode. Device will ask you to select user name you want to use. By returning to the Main Menu, you will see the name of the operator in use. By clicking on the arrow below the name of the operator, you can switch off the FIRST or change operator.
  • Page 19: Units

    2.2.5.5. Units Enable you to change unit of viscosity values. 2.2.5.6. Measuring System Allows you to add or remove a Measuring System. To create a measurement system, the instrument will ask for both constants and the name. You will find below list of measuring system compatible with your device and corresponding constant.
  • Page 20: Locked Mode

    MS ASTM SYSTEM Ktau / 1 mNm in Pa Kd / 1 RPM in S-1 Ri / Ra RV 1 13,91 RV 2 55,65 RV 3 139,1 RV 4 278,2 RV 5 556,5 RV 6 1391 RV 7 5565 LV 1 LV 2 LV 3 1900...
  • Page 21: Miscellaneous

    When you click "Enable", the FIRST will ask you to save a 4-digit code that will be required to disable this protected mode. Each activation is independent and can be done with a different code. The protected mode is indicated by the presence of a padlock-like icon. BUT TO DISABLE THIS LOCKED MODE, YOU SHOULD USE 4-digit CODE USED TO ENABLE IT.
  • Page 22: Density

    2.2.5.9. Density Enable you to enter density value of your product in order to measure his kinematic viscosity. If you set a density value, you will get all the time viscosity in cStoke. Please remove density information if you want to get back Pa.s or Poise for unit of viscosity. 2.2.5.10.
  • Page 23: Service

    Indeed some measuring systems require the installation of accessory before the insertion of the spindle. As the FIRST PLUS LR get only one kind of bayonet coupling system, way to install measuring bob on shaft of viscometer is always the same. You will find below how to install your measuring bob.
  • Page 24: Ms Astm

    3.2. MS ASTM Measuring spindles according to ASTM / ISO 2555 (316L stainless steel). These systems are ideally suited for simple viscosity measurement at controlled rotational speed in all areas of activity. The standard recommends use of 600ml beaker for measurement.
  • Page 25 The spindle L are delivered complete, while the R discs must be screwed on the R1-6 axis (Ref 111000). When measuring, it is strongly recommended to heat the 600ml beaker. You can use either a thermostatic bath or the EVA LR PLUS temperature control system. Place the viscometer on its support (see section 1.5).
  • Page 26: Ms Ulv

    the mark on the axis mobile). Be careful that the tip of the mobile is 10 mm or more from the bottom of the beaker. When the measurement height is optimum, use screw on arm to block height of measuring head.
  • Page 27 Here are the available measuring system: All this part can be combined to create two different measuring system. Diameter Part Volume (mm) Designation Measuring Number Shear rate Viscosity range sample system Measuring range (s-1) (mPa.s) (ml) Int. Ext. system MS-C19(light)-C 116030 1 to 510 1 to 26K...
  • Page 28 If this is not the case, do not force it and contact your local distributor or LAMY RHEOLOGY. When the measuring head is properly positioned, there is no need to lock the position using the screw on the arm. Also, be sure to allow sufficient...
  • Page 29 Once the setup is complete, you can do your measurement by clicking on “Start” (see section 2.2.2). When your measurement is complete, it is recommended to remove the cylinder from the viscometer shaft. It will rest in the tube. Rise the measuring head to the highest position by blocking the stem with the screw provided (see section 1.2).
  • Page 30 Go to section 2.2.2, select spindle, shear rate and time and make a zero. Place the disposable cup holder in the well of the temperature control. Take a disposable cup, fill it with your product (see table on the previous page for the volume of product to be put into the measuring cup).
  • Page 31: Verification Of Your Device

    VERIFICATION OF YOUR DEVICE Your instrument is calibrated at the factory with an ASTM L2 mobile and a certified oil with a viscosity close to 1000 mPa.s. Viscosity measurement on a 1000 mPa.s standard silicon oil with ASTM 2555 L2 measuring system.
  • Page 32 LAMY RHEOLOGY 11 A, rue des Aulnes 69410 Champagne au Mont d'Or (France) Tel : 33 (0)4 78 08 54 06 Fax : 33 (0)4 78 08 69 44 contact@lamyrheology.com...

This manual is also suitable for:

B-one plus lrRm 100 plus

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