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Table of Contents
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Summary of Contents for Buchi B-585
- Page 1 Glass Oven B-585 Operation Manual 096981H en...
- Page 2 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience; espe- cially in respect to structure, illustrations and technical detail. This manual is copyright. Information from it may not be reproduced, distributed, or used for competitive purposes, nor made available to third parties.
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Page 3: Table Of Contents
Declaration of conformance Please read these instructions thoroughly before using the Glass Oven B-585. Keep these instructions in the imme diate vicinity of the device so that they can be referred to at any time. Chapter 2 contains important safety advice. These infor mation is vital to the safe operation of the glass oven. -
Page 4: Scope Of Delivery
Order Code Drying oven B-585 100 V - 230 V / 50/60 Hz 46600 Additional package contents: 2 Replacement fuses 3,15 AT Fig. 1: B-585 Drying 1 Drying accessory complete 37010 1 Mains cable PNE, 1.5m Typ CH 10010 Typ Schuko... -
Page 5: Glass Oven For Ball Tube (Kugelrohr) Distillation
1 Cooling unit compl. c 46616 1 3-wire power cord. 1.5m Type CH 10010 Type Schuko 10016 Type GB 17835 Fig. 5a: Glass Accessories including with B-585 Kugelrohr configuration Type USA 10023 Type AUS 17836 1 Instructions German 96980 English... - Page 6 1 Drying accessory for converting to the Fig. 6a: 10 ml ball tube B-585 Drying model 37010 1 Complete sublimation accessory for converting to the B-585 Sublimation model 37133 1 Freeze drying accessories 46710 Fig. 6b: 40 ml ball tube Fig.
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Page 7: Safety
Glass Oven B-585 2 Safety 2 Safety The device has been built using state art techniques and in ac- cordance with the recognized safety regulations. There are no risks or hazards associated with the use of this device if used according to the instructions. -
Page 8: Improper Use
2 Safety Glass Oven B-585 2.4 Improper use Using the device for any other purpose other than those stated above or using in any application that does not correspond to the technical data is considered to be improper usage. Any damage resulting from such use is the sole responsibility of the operator. -
Page 9: Safety Measures
2 Safety Glass Oven B-585 2.6 Safety measures It is required that you wear protective gear such as pro tective glasses, gloves and a lab coat. These instructions must be available at all times to the operating personnel at the location where the device has been installed, as it is considered to be a component of the glass oven. -
Page 10: Function
3 Function Glass Oven B-585 3 Function 3.1 Working with the glass ovens The core of the glass oven comprises two borosilicate glass tubes lying one within the other. The outer tube (1) protects against damage to the heating tube, and at the same time prevents contact with parts that are electrically live. - Page 11 Glass Oven B-585 3 Function Fig. 7: Function principle of the glass oven a Jacket tube b Heat protection c Heating tube d Temperature sensor The electrically conductive semiconductor layer operates at supply voltage. There is a possibility for fatal injuries when the...
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Page 12: Putting Into Operation
In a vertical operation care must be taken to ensure that every cable of the B-585 not gets in contact with the heating element. Discription of the interface: Drive:... -
Page 13: Operation
- edit - delete OPTIONS CONTRAST VACUUM CONTROL UNIT OF TEMPERATURE LANGUAGE Yes / No °C / ° F 0 - 100% - English - Spanish - German - Italian - French - Japanese Fig. 8: Overview of program structure B-585... -
Page 14: Basic Display Arrangement
5 Operation Glass Oven B-585 5.2. Basic display arrangement a Active mode information b Operating condition c Actual temperature d Temperature unit of measurement e Graphic display of heating intensity f Display of the elapsed time g Set point adjustment... - Page 15 Glass Oven B-585 5 Operation 5.2.1 Operation of the B-585 in manual mode Cchanging the actual temperature and the speed of rotation in manual mode. By pressing the Multifunction botton the user gets into the working menu, where the changes to the actual temperature set point and the rotation speed can be made.
- Page 16 Fahrenheit or °Celsius. On the menu item Vac. pump it is possible to switch the vacuum pump on or off directly from the B-585, (Requires Büchi vacuum pump V-500 series with the B-585/V-500 cable). The cable has to be connected at the plug socket in the middle.
- Page 17 5 Operation Glass Oven B-585 5.2.7 Operation of the B-585 in the program mode Fundamental arrangement of the display: a Information about the active mode and current stage of the program (I, II or III) b Operating condition c Actual temperature...
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Page 18: Operation Of The B-585 Drying
5 Operation Glass Oven B-585 5.3 Operation of the B-585 Drying Oven Please ensure that the device has been correctly put into opera- tion according to Chapter 4, Putting into operation. 5.3.1 Operational and display elements a Unit sockets with main fuses... - Page 19 Glass Oven B-585 5 Operation 5.3.3 Filling with the Material to be Dried The drying accessory consists of three parts. While the drying is in progress, the drying tube a into which the product is put (either directly or inside a container), is in the oven. The end cap b that catches the moisture evaporated off can be filled with desiccants to improve the drying effect.
- Page 20 5 Operation Glass Oven B-585 5.3.4 Placing the Drying Tube in the Drying Oven If the material to be dried has been placed in the drying tube according to Chapter 5..., the tube and the end cap are scre- wed together. The entire assembly is then placed in the drying oven and fastened with the screw a .
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Page 21: Operation Of The B-585 Kugelrohr
Glass Oven B-585 5 Operation 5.4 Operation of the B-585 Kugelrohr Please ensure that the device has been correctly put into opera- tion according to Chapter 4, Putting into operation 5.4.1 Operational and display elements a Unit sockets with main fuses... - Page 22 5 Operation Glass Oven B-585 5.4.3 Cooling For substances with a low boiling point, air-cooling is not always sufficient to make the vapour condense in the balls outside of the oven area. In this case, it is recom men ded to use a cooling appa ratus.
- Page 23 Glass Oven B-585 5 Operation 5.4.5 Working procedure for a simple distillation The liquid to be distilled is placed in the vertical glass tube with having only a single ground-glass joint using a pipette. The glass tube can be filled up to the „max“ mark. The desired number of glass balls are connected to each other and secured against unwanted release with the clips.
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Page 24: Accessories: Sublimation And Freeze Drying
5 Operation Glass Oven B-585 5.4.8 Working procedure for rotation drying The vapor duct used for the ball tube distillation must be remo- ved and the vapour duct for rotation drying installed in order to do rotation drying. See Chapter 5.2.3 for information on how to convert the device. -
Page 25: Converting The Glass Oven Configurations
If the samples is in frozen condition in the freeze drying tube, the B-585 is evacuated. The vacuum which can be chosen depends upon the freezing point of the product. Set a va- cuum pressure, which ensures a product temperature 10 degrees below the melting point during the drying process. - Page 26 5 Operation Glass Oven B-585 5.6.2 From drying to freeze drying The freeze drying accessory is immersed into the drying accessory and the vacuum is put on. 5.6.3 From drying configurationto Kugelrohr configuration First of all switch off the instrument and let it cool down (if it is necessary) Fig.
- Page 27 5 Operation Glass Oven B-585 To install the drive unit, remove the connection (2) at the end of the rods (1), insert the rods into the openings (3) on the glass oven. Fix up the connection (2) again on the rods.
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Page 28: Maintenance
6 Maintenance Glass Oven B-585 6 Maintenance All guidelines which are meant to keep the glass oven in working order should be followed. This also includes a periodic cleaning and checking for any visible damage. 6.1 Cleaning The housing of the B-580 glass oven is coated with paint. Clean only with dry rag or a rag moistened with alcohol. -
Page 29: Taking Out Of Operation
Glass Oven B-585 7 Taking out of operation 7 Taking out of operation The device must be cooled down and thoroughly cleaned. 7.1 Storage/Transport The device must be stored and transported in the original packa- ging, and must be thoroughly clean. -
Page 30: Replacement Parts
Chapter 6, Maintenance. The manu facturing of this product, as described in these in struc - tions, is prohibited. 8.1 B-585 Drying configuration replacement parts complet Nr. 37010 37287 Drying accessory complete... -
Page 31: B-585 Kugelrohr Configuration Replacement Parts
Glass Oven B-585 8 Replacement parts 8.2 B-585 Kugelrohr configuration replacement parts 37118 37286 37073 37102 Description Order Code 37101 10 ml ball tube (Ns 14.5/23) with vapour duct and clips 37118 37107 37106 37286 37073 37104 20ml ball tube (Ns 14.5/23) -
Page 32: Appendix
9 Appendix Glass Oven B-585 9 Appendix 9.1 Technical data Supply voltage 100 - 230 VAC +/-10 % 50/60 Hz Frequency Power max. 450 W Pin assignment Pin 1: Ground (Gnd) Pin 2: + 24 V DC Pin 3 to 8: not assigned ca. -
Page 33: Materials Used
Glass Oven B-585 9 Appendix 9.3 Materials used Description Materials Material code Housing Steel sheet metal ST 12 Heating tube Borosilicate glass Glass jacket tube Borosilicate glass Cooling dish Hard-polyethylene HD-PE Heater fixture (site) Aluminium ALMGSI 1 Kugelrohr-Insert Aluminium ALMGSI 1... -
Page 36: German
T +55 19 3849 1201 F +66 2 862 08 54 F +971 4 313 2861 F +55 19 3849 2907 bacc@buchi.com middleeast@buchi.com latinoamerica@buchi.com www.buchi.com www.buchi.com www.buchi.com We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...
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