Endress+Hauser Analytik Jena multi EA 5100 Manuals

Manuals and User Guides for Endress+Hauser Analytik Jena multi EA 5100. We have 1 Endress+Hauser Analytik Jena multi EA 5100 manual available for free PDF download: Operating Manual

Endress+Hauser Analytik Jena multi EA 5100 Operating Manual (182 pages)

C/N/S/X Analyzer

Brand: Endress+Hauser | Category: Measuring Instruments | Size: 3.76 MB

Table of Contents
3
About this User Manual
7
Intended Use
8
Security
10
Safety Labeling on the Device
10
Requirements for the Operating Personnel
11
Safety Instructions, Transport and Commissioning
11
Safety Instructions: During Operation
12
General Safety Instructions During Operation
12
Safety Instructions - Protection against Explosion and Fire
12
Safety Instructions: Electrical Equipment
13
Handling of Auxiliary and Operating Materials
13
Decontamination after Soiling
14
Behavior During Overpressure Faults (0206, Gas Pressure Fault)
14
Behavior During Emergencies
14
Safety Instructions - Maintenance and Repair
15
Function and Design
16
Multi EA 5100 Basic Module
16
Principle of Operation
16
Figure 1 Operating Modes of the Multi EA 5100
17
Design of the Basic Module
18
Figure 2 Front View in Vertical Operation Mode
19
Figure 3 Basic Module in Horizontal Operation Mode
19
Figure 4 Basic Module with a Sampling Module and a Detection Module
20
Figure 5 Interfaces on the Rear of the Device
21
Figure 6 Power Connection, Power Switch
21
Figure 7 Interfaces for Detector Modules and Sampling Modules
22
Figure 8 Connection for the Sensors and the Combustion Furnace in the Device
22
Figure 9 Connections for the Auto-Protection Valve Assembly and Transfer Line
23
Figure 10 Hose Diagram for Horizontal Operation
24
Figure 11 Hose Diagram for Vertical Operation
25
Figure 12 Gas Connections at the Rear of the Device
26
Figure 13 Gas Connections on the Gas Box
27
Figure 14 Connections on the Combustion Tube
27
Figure 15 Combustion Furnace in the Vertical and Horizontal Operating Mode
28
Figure 16 Multi-Purpose Combustion Tube
28
Sampling Modules
29
Auto-Injector
29
Figure 17 Membrane Dryer
29
Installation and Commissioning
30
Installation Conditions
30
Installation Location Requirements
30
Power Supply
30
Gas Supply
31
Device Layout and Space Requirements
31
Figure 18 Space Required for the Basic Device and Modules (Vertical Operation)
32
Figure 19 Space Required for the Basic Device and Modules (Horizontal Operation)
33
Installing and Commissioning the Analysis System
34
Figure 20 Media Connections of the Rear of the Device
35
Operation
36
General Notes for Measuring Operations
36
Selecting the Measurement Method
37
Switching on the Basic Module and the Modules
38
Switching off the Basic Module and the Modules
39
Recommissioning after Emergency Shutdown (Cl Module 5100)
40
Nitrogen Analysis with the N Module 5100
42
Function and Design
42
Function and Measuring Principle
42
Design
42
Connection
43
Figure 21 Basic Module with Detection Module and Sampling Module
43
Figure 22 Rear of the Nitrogen Detector
44
Installation
45
Figure 23 Absorber
45
Figure 24 Connecting Detection Modules to the Basic Module
46
Operation
47
Chlorine Analysis with the Cl Module 5100
48
Function and Design
48
Function and Measuring Principle
48
Design
48
Figure 25 Design of the Chlorine Detector (Without Measuring Cell)
49
Figure 26 Measuring Cell "Sensitive" with Lid
50
Figure 27 Equipped Measuring Cell
50
Figure 28 Combined Electrode
51
Figure 29 Measuring Cell "High Concentration" with Lid
51
Figure 30 Measuring Cell "High Sensitive" with Lid
52
Figure 31 Lid of the "High Sensitive" Measuring Cell Equipped with All Electrodes
53
Figure 32 Reference Electrode and Sensor Electrode
54
Figure 33 Exhaust Connection
54
Figure 34 Platinum Electrode with Salt Bridge
55
Figure 35 Silver Electrode
55
Connection
56
Figure 36 Rear of the Chlorine Detector
56
Figure 37 Measuring Cell Connections
57
Figure 38 Connection of the Heated Gas Transfer Lines to the Sulfuric Acid Container
57
Figure 39 Gas Infeed Tube with PTFE Connector
58
Figure 40 Gas Infeed to the "Sensitive" Measuring Cell
58
Installation
59
Figure 41 Connection of the Heated Gas Transfer Lines to the Sulfuric Acid Container
60
Figure 42 Connection of the Gas Transfer Line in the Basic Module
61
Operation
63
Preparing the Measuring Cell
63
Operating the Analysis System
65
Notes for Measuring Operations
66
Sulfur Analysis with the S Module 5100 (Basic, MPO)
67
Function and Design
67
Function and Measuring Principle
67
Design
67
Figure 43 Basic Module with Detection Module and Sampling Module
67
Connection
68
Figure 44 Rear of the Sulfur Detector
68
Installation
69
Figure 45 Chemical Ozone Decomposer
69
Operation
70
Sulfur Analysis with the S Module 5100 Coulometric
71
Function and Design
71
Function and Measuring Principle
71
Design
71
Figure 46 Coulometric Sulfur Detector with Measuring Cell (Without Door)
72
Figure 47 Coulometric Sulfur Detectors Without Measuring Cell
73
Figure 48 Coulometric Measuring Cell
74
Figure 49 Generator and Indicator Electrodes, Gas Inlet Tube
75
Figure 50 Nox Absorber and HX Absorber
76
Figure 51 Hose Diagram
76
Connection
77
Installation
77
Figure 52 Rear of the Coulometric Sulfur Detector
77
Figure 53 Coulometric Sulfur Detector with Measuring Cell (Without Door)
79
Operation
80
Preparing the Measuring Cell
80
Operating the Analysis System
81
Carbon Analysis with the C Module 5100
83
Function and Design
83
Function and Measuring Principle
83
Design
83
Figure 54 Basic Module with Detection Module and Sampling Module
83
Connection
84
Figure 55 Rear of the Carbon Detector
84
Installation
85
Operating the Analysis System
85
Carbon Analysis with the TOC Module 5100
87
Function and Design
87
Function and Measuring Principle
87
Design
87
Figure 56 TOC Detector, Door Opened
88
Figure 57 Components in the Basic Module
89
Figure 58 TOC Combustion Tube (Unfilled)
89
Figure 59 Tube Holder for the TOC Combustion Tube
90
Figure 60 Condensation Coil
91
Connection
92
Figure 61 Hose Diagram of the TOC Detector
92
Figure 62 Rear of the TOC Detector
93
Installation
94
Figure 63 TOC Detector, Door Opened
95
Operation
96
Operating the Analysis System
96
Figure 64 TOC Combustion Tube
96
Notes for Measuring Operations
97
Troubleshooting
98
General Notes
98
Remedying Software Message Faults
98
Initializing the Basic Module and the System Components
104
Displays in the Window Status Analyzer
105
Overview
105
Figure 65 Status Analyzer Window
105
Method
106
Sampling Modules
106
Detectors
107
Device Faults on the Basic Module
109
Analytical Problems in the Basic Module
111
Device Faults on the N Module 5100
112
Analytical Problems During TC Determination
113
Device Faults on the Chlorine Detector
114
Analytical Problems During AOX, EOX and TX Determination
115
Device Faults on the S Module 5100 Basic and S Module 5100 MPO
116
Analytical Problems During TS Determination
116
Device Faults on the Coulometric Sulfur Detector
117
Analytical Problems During Coulometric TS Determination
117
Device Faults on the Carbon Detector
119
Analytical Problems During TC, EC/OC Determination
119
Device Faults on the TOC Detector
120
Analytical Problems During TC, EC/OC, TOC, NPOC and TIC Determination
121
Maintenance and Care
124
Overview of Maintenance Work
124
Maintenance of the Multi-Purpose Combustion Tube
126
Removing the Combustion Tube
127
Cleaning the Combustion Tube
128
Inserting the Quartz Wool Plug
128
Installing the Combustion Tube
129
Maintenance of the Auto-Protection Valve Assembly
131
Installing/Removing the Auto-Protection Valve Assembly
131
Check and Replace the Filter
132
Replacing the Pneumatic Seal
133
Replacing the Membrane Dryer
134
Replacing the Hose Connections
136
Replacing the Septum on the Injection Port
136
Figure 66 Replacing the Fingertight Connections
136
Figure 67 Replacing the Septum on the Injection Port of the Combustion Tube
136
Replacing the Check Valves and Particle Filters
137
Replacing the Check Valves on the Gas Box
137
Replacing the Particle Filters in the Gas Inlets
138
Checking the System for Leaks
139
System Tightness for N/S/C Methods
139
System Tightness for Cl Methods
139
System Tightness for TOC Methods
141
Removing and Installing the Combustion Furnace
141
Maintenance of the N Module 5100 Nitrogen Detector
143
Replacing the Ozone Generator
143
Figure 68 Replacing the Ozone Generator
144
Replacing the Absorber
145
Figure 69 Absorber
145
Replacing the Chemical Ozone Decomposer
146
Maintenance of the Cl Module 5100 Chlorine Detector
147
Replacing the Sulfuric Acid and Cleaning the Sulfuric Acid Container
147
Figure 70 Replacing the Chemical Ozone Decomposer
147
Figure 71 Connection of the Heated Gas Transfer Lines to the Sulfuric Acid Container
148
Maintenance of the Measuring Cell
149
Maintenance and Storage of the Electrodes
150
Figure 72 Correct Handling of the Combined Electrode
150
Maintenance of the S Module 5100 Basic and S Module 5100 MPO Sulfur Detector
152
Replacing the UV Lamp
152
Replacing the Chemical Ozone Decomposer
154
Figure 73 Replacing the Chemical Ozone Decomposer
154
Maintenance of the Coulometric Sulfur Detector
155
Replacing the Absorber
155
Figure 74 Nox Absorber and HX Absorber
156
Replacing the Electrolyte Solution
157
Figure 75 Coulometric Sulfur Detector with Measuring Cell (Without Door)
157
Maintenance of the TOC Detector
158
Replacing the Water Traps
159
Replacing the Halogen Trap
159
Figure 76 Replace the Water Traps
159
Figure 77 Replacing the Halogen Trap
160
Regenerating the TIC Reactor
161
Cleaning the TIC Reactor
161
Figure 78 TOC Detector, Door Opened
162
Replacing the Pump Hose of the Condensate Pump
163
Figure 79 Installing the Pump Hose in the Guide Piece
163
Cleaning the Condensation Coil
164
Figure 80 Components in the Basic Module
164
Replacing the Catalyst in the TOC Combustion Tube
165
Figure 81 TOC Combustion Tube
166
Transport and Storage
167
Transport
167
Moving the Device in the Laboratory
167
Storage
167
Preparing the Basic Module for Transport and Storage
168
Preparing Detection Modules
168
Notes for the Transport of the Cl Module 5100
169
Notes on Transport of the S Module 5100 Coulometric
170
Notes on Transport of the TOC Module 5100
170
Disposal
171
Specifications
172
Technical Data for the Multi EA 5100
172
Technical Data of the N Module 5100
176
Technical Data for the Cl Module 5100
176
Technical Data for the S Module 5100 (Basic, MPO)
177
Technical Data for the S Module 5100 Coulometric
178
Technical Data for the C Module 5100
178
Technical Data for the TOC Module 5100
179
Standards and Directives
180

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Endress+Hauser Analytik Jena multi EA 5100 Operating Manual (182 pages)

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