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Analytik Jena multi EA 5000
Endress+Hauser Analytik Jena multi EA 5000 Manuals
Manuals and User Guides for Endress+Hauser Analytik Jena multi EA 5000. We have
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Endress+Hauser Analytik Jena multi EA 5000 manual available for free PDF download: Operating Manual
Endress+Hauser Analytik Jena multi EA 5000 Operating Manual (186 pages)
C/N/S/X Analyzer
Brand:
Endress+Hauser
| Category:
Measuring Instruments
| Size: 3.78 MB
Table of Contents
Table of Contents
3
1 About this User Manual
7
2 Intended Use
8
3 Security
10
Safety Labeling on the Device
10
Requirements for the Operating Personnel
11
Safety Instructions, Transport and Commissioning
11
Safety Instructions: During Operation
12
General Safety Instructions During Operation
12
Safety Instructions - Protection against Explosion and Fire
12
Safety Instructions: Electrical Equipment
13
Handling of Auxiliary and Operating Materials
13
Decontamination after Soiling
14
Behavior During Overpressure Faults (0206, Gas Pressure Fault)
14
Behavior During Emergencies
14
Safety Instructions - Maintenance and Repair
15
4 Function and Design
16
Multi EA 5000 Basic Module
16
Principle of Operation
16
Figure 1 Operating Modes of the Multi EA 5000
17
Design of the Basic Module
18
Figure 2 Front View in Vertical Operation Mode
19
Figure 3 Basic Module in Horizontal Operation Mode
19
Figure 4 Basic Module with a Sampling Module and a Detection Module
20
Figure 5 Interfaces on the Rear of the Device
21
Figure 6 Power Connection, Power Switch
21
Figure 7 Interfaces for Detector Modules and Sampling Modules
22
Figure 8 Connection for the Sensors and the Combustion Furnace in the Device
22
Figure 9 Connections for the Auto-Protection Valve Assembly and Transfer Line
23
Figure 10 Hose Diagram for Horizontal Operation
24
Figure 11 Hose Diagram for Vertical Operation
25
Figure 12 Gas Connections at the Rear of the Device
26
Figure 13 Gas Connections on the Gas Box
27
Figure 14 Connections on the Combustion Tube
27
Figure 15 Combustion Furnace in the Vertical and Horizontal Operating Mode
28
Figure 16 Multi-Purpose Combustion Tube
28
Sampling Modules
29
Auto-Injector
29
Figure 17 Membrane Dryer
29
Manual Boat Drive (MBD)
30
5 Installation and Commissioning
31
Installation Conditions
31
Installation Location Requirements
31
Power Supply
31
Gas Supply
32
Device Layout and Space Requirements
32
Figure 18 Space Required for the Basic Device and Modules (Vertical Operation)
33
Figure 19 Space Required for the Basic Device and Modules (Horizontal Operation)
34
Installing and Commissioning the Analysis System
35
Figure 20 Media Connections of the Rear of the Device
36
6 Operation
37
General Notes for Measuring Operations
37
Selecting the Measurement Method
38
Switching on the Basic Module and the Modules
39
Switching off the Basic Module and the Modules
40
Recommissioning after Emergency Shutdown (Cl Module)
41
7 Nitrogen Analysis with the CLD 5000
43
Function and Design
43
Function and Measuring Principle
43
Design
43
Connection
44
Figure 21 Basic Module with Detection Module and Sampling Module
44
Figure 22 Rear of the Nitrogen Detector
45
Installation
46
Figure 23 Absorber
46
Figure 24 Connecting Detection Modules to the Basic Module
47
Operation
48
8 Chlorine Analysis with the Cl Module
49
Function and Design
49
Function and Measuring Principle
49
Design
49
Figure 25 Design of the Chlorine Detector (Without Measuring Cell)
50
Figure 26 Measuring Cell "Sensitive" with Lid
51
Figure 27 Equipped Measuring Cell
51
Figure 28 Combined Electrode
52
Figure 29 Measuring Cell "High Concentration" with Lid
52
Figure 30 Measuring Cell "High Sensitive" with Lid
53
Figure 31 Equipped Measuring Cell
54
Figure 32 Sensor Electrode
55
Figure 33 Exhaust Connection
55
Figure 34 Platinum Electrode with Salt Bridge
56
Figure 35 Silver Electrode
56
Connection
57
Figure 36 Rear of the Chlorine Detector
57
Figure 37 Measuring Cell Connections
58
Figure 38 Connection of the Heated Gas Transfer Lines to the Sulfuric Acid Container
58
Figure 39 Gas Infeed Tube with PTFE Connector
59
Figure 40 Gas Infeed to the "Sensitive" Measuring Cell
59
Installation
60
Figure 41 Connection of the Heated Gas Transfer Lines to the Sulfuric Acid Container
61
Figure 42 Connection of the Gas Transfer Line in the Basic Module
62
Operation
64
Preparing the Measuring Cell
64
Operating the Analysis System
66
Notes for Measuring Operations
67
9 Sulfur Analysis with the UVFD 5000, MPO 5000
69
Function and Design
69
Function and Measuring Principle
69
Design
69
Figure 43 Basic Module with Detection Module and Sampling Module
69
Connection
70
Installation
71
Figure 44 Rear of the Sulfur Detector
71
Figure 45 Chemical Ozone Decomposer
72
Operation
73
10 Sulfur Analysis with the Coulometric Sulfur Module
74
Function and Design
74
Function and Measuring Principle
74
Design
74
Figure 46 Coulometric Sulfur Detector with Measuring Cell (Without Door)
75
Figure 47 Coulometric Sulfur Detectors Without Measuring Cell
76
Figure 48 Coulometric Measuring Cell
77
Figure 49 Generator and Indicator Electrodes, Gas Inlet Tube
78
Figure 50 Nox Absorber and HX Absorber
79
Figure 51 Hose Diagram
79
Connection
80
Figure 52 Rear of the Coulometric Sulfur Detector
80
Installation
81
Figure 53 Coulometric Sulfur Detector with Measuring Cell (Without Door)
82
Operation
83
Preparing the Measuring Cell
83
Operating the Analysis System
84
11 Carbon Analysis with the TC Module
86
Function and Design
86
Function and Measuring Principle
86
Design
86
Figure 54 Basic Module with Detection Module and Sampling Module
86
Connection
87
Figure 55 Rear of the Carbon Detector
87
Installation
88
Operating the Analysis System
88
12 Carbon Analysis with the TOC Module
90
Function and Design
90
Function and Measuring Principle
90
Design
90
Figure 56 TOC Detector, Door Opened
91
Figure 57 Components in the Basic Module
92
Figure 58 TOC Combustion Tube (Unfilled)
92
Figure 59 Tube Holder for the TOC Combustion Tube
93
Figure 60 Condensation Coil
94
Connection
95
Figure 61 Hose Diagram of the TOC Detector
95
Figure 62 Rear of the TOC Detector
96
Installation
97
Figure 63 TOC Detector, Door Opened
98
Operation
99
Operating the Analysis System
99
Figure 64 TOC Combustion Tube
99
Notes for Measuring Operations
100
13 Troubleshooting
101
General Notes
101
Remedying Software Message Faults
101
Initializing the Basic Module and the System Components
107
Displays in the Window Status Analyzer
108
Overview
108
Figure 65 Status Analyzer Window
108
Method
109
Sampling Modules
109
Detectors
110
Device Faults on the Basic Module
112
Analytical Problems in the Basic Module
114
Device Faults on the CLD 5000
115
Analytical Problems During TC Determination
116
Device Faults on the Chlorine Detector
117
Analytical Problems During AOX, EOX and TX Determination
118
Device Faults on the UVFD 5000 and MPO 5000
119
Analytical Problems During TS Determination
119
Device Faults on the Coulometric Sulfur Detector
120
Analytical Problems During Coulometric TS Determination
120
Device Faults on the Carbon Detector
122
Analytical Problems During TC, EC/OC Determination
122
Device Faults on the TOC Detector
123
Analytical Problems During TC, EC/OC, TOC, NPOC and TIC Determination
124
14 Maintenance and Care
127
Overview of Maintenance Work
127
Maintenance of the Multi-Purpose Combustion Tube
129
Removing the Combustion Tube
130
Cleaning the Combustion Tube
131
Inserting the Quartz Wool Plug
131
Installing the Combustion Tube
132
Maintenance of the Auto-Protection Valve Assembly
134
Installing/Removing the Auto-Protection Valve Assembly
134
Check and Replace the Filter
135
Replacing the Pneumatic Seal
136
Replacing the Membrane Dryer
137
Replacing the Hose Connections
139
Replacing the Septum on the Injection Port
139
Figure 66 Replacing the Fingertight Connections
139
Figure 67 Replacing the Septum on the Injection Port of the Combustion Tube
139
Replacing the Check Valves and Particle Filters
140
Replacing the Check Valves on the Gas Box
140
Replacing the Particle Filters in the Gas Inlets
141
Checking the System for Leaks
142
System Tightness for N/S/C Methods
142
System Tightness for Cl Methods
142
System Tightness for TOC Methods
144
Removing and Installing the Combustion Furnace
144
Maintenance of the CLD 5000 Nitrogen Detector
146
Replacing the Ozone Generator
146
Replacing the Absorber
148
Figure 68 Replacing the Ozone Generator
148
Replacing the Chemical Ozone Decomposer
149
Figure 69 Absorber
149
Figure 70 Replacing the Chemical Ozone Decomposer
150
Maintenance of the Cl Module Chlorine Detector
151
Replacing the Sulfuric Acid and Cleaning the Sulfuric Acid Container
151
Figure 71 Connection of the Heated Gas Transfer Lines to the Sulfuric Acid Container
151
Maintenance of the Measuring Cell
152
Maintenance and Storage of the Electrodes
153
Figure 72 Correct Handling of the Combined Electrode
154
Maintenance of the UVFD 5000 and MPO 5000 Sulfur Detector
156
Replacing the UV Lamp
156
Replacing the Chemical Ozone Decomposer
158
Figure 73 Replacing the Chemical Ozone Decomposer
158
Maintenance of the Coulometric Sulfur Detector
159
Replacing the Absorber
159
Figure 74 Nox Absorber and HX Absorber
160
Replacing the Electrolyte Solution
161
Figure 75 Coulometric Sulfur Detector with Measuring Cell (Without Door)
161
Maintenance of the TOC Detector
162
Replacing the Water Traps
163
Replacing the Halogen Trap
163
Figure 76 Replace the Water Traps
163
Figure 77 Replacing the Halogen Trap
164
Regenerating the TIC Reactor
165
Cleaning the TIC Reactor
165
Figure 78 TOC Detector, Door Opened
166
Replacing the Pump Hose of the Condensate Pump
167
Figure 79 Installing the Pump Hose in the Guide Piece
167
Cleaning the Condensation Coil
168
Figure 80 Components in the Basic Module
168
Replacing the Catalyst in the TOC Combustion Tube
169
Figure 81 TOC Combustion Tube
170
15 Transport and Storage
171
Transport
171
Moving the Device in the Laboratory
171
Storage
171
Preparing the Basic Module for Transport and Storage
172
Preparing Detection Modules
172
Notes for the Transport of the Cl Module
173
Notes on Transport of the Coulometric Sulfur Module
174
Notes on Transport of the TOC Module
174
16 Disposal
175
17 Specifications
176
Technical Data for the Multi EA 5000
176
Technical Data of the CLD 5000
180
Technical Data for the Cl Module
180
Technical Data for the UVFD 5000, MPO 5000
181
Technical Data for the Coulometric Sulfur Module
182
Technical Data for the TC Module
182
Technical Data for the TOC Module
183
Standards and Directives
184
Table of Figures
185
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