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HP 5973 Hardware Installation Manual

Mass selective detector
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HP 5973
Mass Selective Detector
Hardware Installation Manual

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Summary of Contents for HP 5973

  • Page 1 ® HP 5973 Mass Selective Detector Hardware Installation Manual...
  • Page 2 Hewlett-Packard Company Deutsch Cautions Safety class LpA << 70 dB am Arbeitsplatz Cautions call attention to The HP 5973 Mass Selective All Rights Reserved. normaler Betrieb nach EN procedures which, if not Detector (MSD) is a Safety Reproduction, adaptation, or...

  • Page 3: Table Of Contents

    Contents Chapter 1 General Information Introduction, 6 Customer responsibilities, 8 Site requirements, 9 Space requirements, 9 Telephone, 9 Environmental requirements, 9 Power requirements, 10 Gases, 10 Other documentation, 13 Chapter 2 Installation Installation, 16 Inspecting the shipped materials, 17 Installing the GC, 18 Installing the MSD, 22 Plumbing the methane line to the CI MSD flow module, 26 Installing the MSD ChemStation, 28...

  • Page 5: General Information

    Introduction, 6 Customer responsibilities, 8 Site requirements, 9 Other documentation, 13 General Information...

  • Page 6: Introduction

    Packard service representative. The HP 5973 MSD system consists of: • Mass Selective Detector HP G1098A — Vapor diffusion pump version of the HP 5973 MSD (“Diffusion pump MSD”) HP G1099A — Turbo molecular pump version of the HP 5973 MSD (“Turbo pump MSD”)
  • Page 7 HP 7983 ALS tower HP 7983 ALS tray HP 5973 MSD HP 5973 MSD system HP 6890 Plus GC HP 7983 ALS tower HP 7983 ALS tray CI flow control module HP 5973 CI MSD HP 5973 CI MSD system...

  • Page 8: Customer Responsibilities

    • Hose for venting pump exhaust outside or to a fume hood, if toxic chemicals will be analyzed or if dangerous carrier or CI reagent gases will be used. • Installation and testing of additional detectors on the HP 6890 Series GC • Training for programs not specifically listed in this document •...

  • Page 9: Site Requirements

    A telephone with a cord long enough to be used at the computer will allow the MSD operator to communicate with HP support personnel. In addition, a second, analog phone line is strongly recommended to allow remote control and diagnosis of the MSD through a modem.

  • Page 10: Power Requirements

     General Information 6LWH UHTXLUHPHQWV Power requirements If possible, all components should be connected to the same line voltage supply circuit. This avoids voltage differences between components. All circuits must have a common ground. Grounding The three-conductor power outlet provided for the MSD must conform to the International Electrotechnical Commission (IEC) requirement for grounding of electrical instruments.
  • Page 11 30.3 3,164 HP 6890 Plus GC 58.5 2,250 8,100 Fast heating oven 2,950 10,620 HP 6890 Series ALS HP 7683 Injector (above GC) HP 7683 Tray (left of GC) 30.3 Height Width Depth Weight Power Heat Instrument (inches) (inches) (inches)
  • Page 12 The following reagent gases and hardware may be required for operation of the CI HP 5973 MSD (depending on your choice of reagent). Always use the highest purity gases available. The hardware items listed below are available from Matheson and Swagelok.

  • Page 13: Other Documentation

    2WKHU GRFXPHQWDWLRQ Other documentation Additional information is contained in the following documentation: • HP 5973 MSD Hardware Manual and online help • HP MSD ChemStation manuals and online help • HP 5973 MSD Reference Collection CD-ROM set • HP 6890 Series GC manuals and online help •...
  • Page 15 Inspecting the shipped materials, 17 Installing the GC, 18 Installing the MSD, 22 Plumbing the methane line to the CI MSD flow module, 26 Installing the MSD ChemStation, 28 Integrating the GC, MSD, and ChemStation, 29 Verifying EI system performance, 30 Switching from EI to CI operating mode, 31 Verifying CI performance, 32 Familiarizing the customer, 33...

  • Page 16: Installation

    Installation This chapter contains instructions for installing the HP 5973 MSD system. Installation of any MSD system includes the following steps: • Inspection of shipped materials • GC installation and preparation • MSD installation • Data system installation • GC and MSD integration •...

  • Page 17: Inspecting The Shipped Materials

    Shipping containers should not be opened until a Hewlett-Packard representative is present to verify the contents of each container. Warranty claims for missing items will not be honored unless an HP representative verifies the contents of each shipping container as it is unpacked.

  • Page 18: Installing The Gc

     Installation ,QVWDOOLQJ WKH *& Installing the GC Materials needed: Column cutter (5181-8836) Flat-blade screwdriver Wrenches, 7/16 inch, open-ended (2 needed) (8710-0806 Please refer to the GC/MS application note, Optimizing splitless injections on your GC for high-performance MS analysis before installing the GC. 1 9HULI\ WKH HOHFWULFDO RXWOHW LV VXLWDEOH IRU WKH *&...
  • Page 19 12 7XUQ RQ WKH *& DQG YHULI\ WKDW WKH *& SDVVHV VHOI WHVW Keep the GC oven turned off. 13 6HW WKH +3,% DGGUHVV LQ WKH *& WR  On the GC keypad, select Options/Communication/HP-IB address/15/ and then press Enter 14 &RQILJXUH WKH FROXPQ SDUDPHWHUV IRU WKH 06' FROXPQ WKDW LV LQVWDOOHG LQ...
  • Page 20  Installation ,QVWDOOLQJ WKH *& 17 5HPRYH WKH VHSWXP FRYHULQJ WKH IUHH HQG RI WKH *& FROXPQ DQG FXW DERXW  FP RII WKH HQG RI WKH FROXPQ Place the free end of the column into a beaker of solvent and check for bubbles to verify helium flow.
  • Page 21  Installation ,QVWDOOLQJ WKH *& Metal knockout Plastic knockouts GC/MSD interface heater cable (GC end)

  • Page 22: Installing The Msd

    ,QVWDOOLQJ WKH 06' Installing the MSD Materials needed: HP 5973 MSD Hardware Manual (G1099-90001) HP 5973 MSD Hardware Manual Supplement (G1099-90009) HP 5973 MSD PCI/NCI Hardware Manual (G1999-90001) Tygon tubing or hose for pump exhaust Wrench, 1/4-inch × 5/16-inch open end (8710-0510)
  • Page 23 7 /RRVHQ WKH UHDU VLGHSODWH WKXPEVFUHZ FRPSOHWHO\ Rear sideplate thumbscrew (loosen completely) 8 9HULI\ WKH +3,% DGGUHVV RQ WKH +3,%06' FRQWURO FDUG LV VHW WR  Remote start cable HP-IB address switch MSD power cord receptacle Foreline pump power cord HP-IB cable...
  • Page 24  Installation ,QVWDOOLQJ WKH 06' 9 &RQQHFW WKH 06' HQG RI WKH *&06' LQWHUIDFH FDEOH WR WKH *& HQG RI WKH *&06' LQWHUIDFH FDEOH HP 6890 Series GC HP 5973 MSD GC/MSD interface cable (MSD end) GC/MSD interface cable (GC end) 10 &RQQHFW WKH +3,% FDEOH IURP WKH *&...
  • Page 25 MSD hardware manual. The column installation tool is located in a clear plastic tube in the MSD tool kit. 21 3XPS GRZQ WKH 06' See the revised procedure in the HP 5973 MSD Hardware Manual Supplement. 22 5HLQVWDOO WKH WRS FRYHU...

  • Page 26: Plumbing The Methane Line To The Ci Msd Flow Module

    3OXPELQJ WKH PHWKDQH OLQH WR WKH &, 06' IORZ PRGXOH Plumbing the methane line to the CI MSD flow module Special procedure for Refer to the HP 5973 MSD PCI/NCI Hardware Manual (G1999-90001) CI MSD Materials needed: Methane supply with regulator...
  • Page 27  Installation 3OXPELQJ WKH PHWKDQH OLQH WR WKH &, 06' IORZ PRGXOH 8 &RQQHFW WKH RWKHU HQG RI WKH WXELQJ WR WKH *DV $ ILWWLQJ RQ WKH IORZ PRGXOH 9 ,I DQRWKHU UHDJHQW JDV LV WR EH XVHG FRQQHFW LW WR WKH *DV % ILWWLQJ If you are going to connect isobutane, you will need another gas purifier for the Gas B line.

  • Page 28: Installing The Msd Chemstation

    See the printer installation documentation. 6 ,QVWDOO WKH PRGHP See the modem installation manual. Not all ChemStations have modems supplied. 7 7XUQ RQ WKH PRGHP SULQWHU PRQLWRU DQG 3& LQ WKDW RUGHU HP-IB cable Remote start cable ALS tray cable ALS tower cable...

  • Page 29: Integrating The Gc, Msd, And Chemstation

     Installation ,QWHJUDWLQJ WKH *& 06' DQG &KHP6WDWLRQ Integrating the GC, MSD, and ChemStation Materials needed: MSD ChemStation software installation manual (G1701-90031) 1 6WDUW XS WKH &DUERQ &RS\ VRIWZDUH DQG FRQILJXUH WKH PRGHP LI \RXU &KHP6WDWLRQ LQFOXGHV D PRGHP 2 ,Q WKH 3URGXFWLYLW\ 7RROV JURXS FOLFN WKH 06 &RQILJ LFRQ DQG FRQILJXUH WKH 06' DQG *&...

  • Page 30: Verifying Ei System Performance

    3 ,Q WKH ,QVWUXPHQW &RQWURO YLHZ VHOHFW Sensitivity Check IURP WKH 4XDOLI\ PHQX The software will load and resolve the method C:\HPCHEM\1\5973\OFN_SN.M. 4 &OLFN WKH DSSURSULDWH LFRQV LQ WKH ,QVWUXPHQW | (GLW ZLQGRZ WR HGLW WKH PHWKRG IRU WKH W\SH RI LQMHFWLRQ 5 &OLFN...

  • Page 31: Switching From Ei To Ci Operating Mode

    Electrostatic discharges to analyzer components are conducted to the side board where they can damage sensitive components. Wear a grounded anti-static wrist strap (see page 98 of the HP 5973 MSD Hardware Manual) and take other anti-static precautions EHIRUH you open the vacuum manifold.

  • Page 32: Verifying Ci Performance

     Installation 9HULI\LQJ &, SHUIRUPDQFH Verifying CI performance Special procedure for Refer to the HP 5973 MSD PCI/NCI Hardware Manual (G1999-90001) CI MSD 1 Perform a positive CI autotune. 6HH SDJH  RI WKH 06' &, KDUGZDUH PDQXDO 2 Verify positive CI performance. 6HH SDJH  RI WKH 06' &, KDUGZDUH PDQXDO Verify that rms signal-to-noise ratio is at least 75:1.

  • Page 33: Familiarizing The Customer

    PCINH3.U. • The gas purifier can not be used with ammonia. • Must ballast foreline pump daily if running ammonia Refer to the maintenance chapter of the 5973 MSD CI manual.

  • Page 35: Checklists

    Installation checklist, 36 Customer familiarization checklist, 40 Checklists...

  • Page 36: Installation Checklist

     Checklists ,QVWDOODWLRQ FKHFNOLVW Installation checklist Inspection of shipped materials o Shipping containers must be opened only with a Hewlett-Packard representative is present to verify the contents of each container. o Check each item off on the packing list, and verify serial numbers. o Record the serial numbers in the installation documentation.
  • Page 37 GC plugged in and turned on o Verify that the GC passes self test o HP-IB address in the GC set to 15 o Column parameters configured o Carrier gas line pressure set to approximately 50 psi (345 KPa)
  • Page 38 Rear side plate thumbscrew loosened completely o GC/MSD interface heater cable connected o HP-IB address on the back of the MSD is set to 20 o HP-IB and remote cables from the GC to the MSD connected o Methane/isobutane gas purifier installed and purged (CI MSD only)
  • Page 39 PCI autotune performed o PCI sensitivity verified o NCI autotune performed o NCI sensitivity verified Instrument log book entries completed Signal-to-noise results faxed or mailed to the factory HP 5973 MSD serial number EI S/N (rms) PCI S/N (rms) NCI S/N (rms)

  • Page 40: Customer Familiarization Checklist

    &XVWRPHU IDPLOLDUL]DWLRQ FKHFNOLVW Customer familiarization checklist The purpose of customer familiarization is to demonstrate the steps required to: • Perform a basic analysis using an HP standard sample • Evaluate the acquired data • Perform routine maintenance Much of the familiarization is accomplished while the hardware is being installed and checked out.
  • Page 41  Checklists &XVWRPHU IDPLOLDUL]DWLRQ FKHFNOLVW Hardware overview o MSD o CI MSD (if applicable) o Gas chromatograph o ALS (if applicable) o Barcode reader (if applicable) o PC hardware and peripherals System operation o Switching on instruments, PC, and peripherals o Starting Windows NT 4.0 and using online help o Starting MSD ChemStation software o Switching between EI and CI operation (CI MSD only)
  • Page 42  Checklists &XVWRPHU IDPLOLDUL]DWLRQ FKHFNOLVW Methods o Edit entire method demonstrated with OFN_SN.M, explaining the GC and MS Scan Parameters. o Scan and SIM acquisition modes described o Data file naming demonstrated o Method save demonstrated o Data acquisition demonstrated while running the signal-to-noise test for customer o Snapshot demonstrated Data analysis...
  • Page 43 Tune charts under Qualify menu demonstrated o Online help for troubleshooting demonstrated Additional support information o Use the manuals, online help and HP MSD Reference Collection CD explained o HP support services and how to obtain help explained — Hardware —...
  • Page 45 GC oven. Study the Hydro- shift fuses or the short-circuit- gen Carrier Gas Safety Guide ing of fuse holders creates a (HP Part No. 5955-5398) before shock hazard for the operator operating the MSD with hydro- and can damage the instru- gen carrier gas.
  • Page 46 ®         Manual Part Number Copyright © 1998 G1099-90006 Hewlett-Packard Printed in USA 1/98...

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