Agilent Technologies 5977C HES MSD Manuals

Manuals and User Guides for Agilent Technologies 5977C HES MSD. We have 1 Agilent Technologies 5977C HES MSD manual available for free PDF download: Operating Manual

Agilent Technologies 5977C HES MSD Operating Manual (234 pages)

Brand: Agilent Technologies | Category: Security Sensors | Size: 15.46 MB

About this Manual
3
Where to Find more Information
4
Table of Contents
5
Introduction
11
5977C Series MSD Version
12
Abbreviations Used
13
The 5977C Series MSD
15
Physical Description
15
Vacuum Gauge
16
MSD Hardware Description
17
Important Safety Warnings
19
Many Internal Parts of the MSD Carry Dangerous Voltages
19
Electrostatic Discharge Is a Threat to MSD Electronics
20
Many Parts Are Dangerously Hot
20
The Oil Pan under the Foreline Pump Can be a Fire Hazard
21
Hydrogen Safety
22
GC Precautions
22
Dangers Unique to GC/MSD Operation
23
Hydrogen Accumulation in an MSD
23
Precautions
24
Safety and Regulatory Certifications
28
Information
29
Symbols
29
Electromagnetic Compatibility
30
Sound Emission Declaration
30
Intended Use
31
Cleaning/Recycling the Product
31
Accidental Liquid Spillage
31
Moving or Storing the MSD
31
To Replace the Primary Fuses
32
Installing 8890 GC Columns
35
Columns
36
Conditioning Columns
36
Conditioning Ferrules
37
Tips and Hints
37
To Install a Capillary Column in a Split/Splitless Inlet
38
To Condition a Capillary Column
41
To Install a Capillary Column in the GC/MSD Interface Using the Self-Tightening Column Nut
42
To Install a Capillary Column in the GC/MSD Interface Using a Standard Column Nut
47
Nut
47
To Install the GC/MSD Interface Tip Seal
50
The GC/MSD Interface for an 8890 Series GC
52
Installing Intuvo 9000 GC Columns
55
Columns
56
Conditioning Columns
57
Tips and Hints
57
To Replace an Intuvo GC Column
59
To Replace an Intuvo 9000 GC Gasket
63
To Install a Column Guard or Jumper Chip
64
To Replace the 9000 GC/MS Tail
68
To Condition an Intuvo Capillary Column
72
To Install the GC/MSD Interface Tip Seal
74
The GC/MSD Interface for a 9000 Series GC
76
Operating in EI Mode
77
Operating the MSD from the DS
79
Configuring the MSD through the Web User Interface (WUI)
80
To Change the Network Settings of the MSD
80
Emodule Mini Display Readout
83
Front Panel Instrument Status LED
84
Before You Turn on the MSD
85
Pumping down
86
Controlling Temperatures
86
Controlling Column Flow
87
Controlling Jetclean Hydrogen Flow
87
Venting the MSD
88
To View MSD Temperature and Vacuum in Manual Tune
89
To Set Monitors for MSD Temperature and Vacuum Status
91
To Set Analyzer Temperatures from the Instrument Control View
94
To Set the GC/MSD Interface Temperature from Masshunter
96
To Monitor High Vacuum Pressure
98
To Tune the MSD in EI Mode
100
To Set the Operation Mode for the Optional Jetclean System
102
To Set the Jetclean Parameters for the Clean Only Mode
103
To Verify EI System Performance
104
To Perform High-Mass Testing
105
To Open the MSD Covers
108
To Vent the MSD
109
To Pumpdown the MSD
112
Operating in CI Mode
115
General Guidelines
116
CI Autotune
117
To Operate the CI MSD
119
To Pumpdown the MSD in CI Mode
120
To Set up the Software for CI Operation
121
To Operate the Reagent Gas Flow Control Module
123
To Set up Methane Reagent Gas Flow
126
To Use Other Reagent Gases
128
To Perform a PCI Autotune (Methane Only)
131
To Perform an NCI Autotune (Methane Reagent Gas)
133
To Verify PCI Performance
135
To Verify NCI Performance
136
To Monitor CI Mode High Vacuum Pressure
137
General Maintenance
139
Before Starting
141
Maintaining the Vacuum System
146
Maintaining the Analyzer
147
To Open the Analyzer Chamber
149
To Remove the EI HES
151
To Connect/Disconnect Wiring to the EI HES
153
To Disassemble the EI HES
154
To Clean the EI HES
157
To Assemble the EI HES
160
To Remove the EI HES Filaments
165
To Install the EI HES Filament
167
To Install the EI HES
168
To Remove the EI XTR, SS, Inert, or HydroNert Source
169
To Connect/Disconnect Wiring from the EI XTR, SS, and Inert Sources
170
To Connect/Disconnect Wiring from the EI Hydro Nert Source
171
To Connect/Disconnect Wiring from the EI HydroNert Source
171
To Disassemble the EI SS or EI Inert Source
172
To Disassemble the EI XTR Source
175
To Disassemble the EI HydroNert Source
178
To Clean an EI XTR, SS, or Inert Source
181
To Clean the EI HydroNert Source
185
To Assemble an EI SS or Inert Source
188
To Assemble the EI XTR Source
191
To Assemble the EI HydroNert Source
194
To Replace a Filament in an EI XTR, SS, Inert, or HydroNert Source
197
Source
199
To Install the EI XTR, SS, Inert, or HydroNert Source
199
To Replace the Electron Multiplier Horn
200
To Close the Analyzer Chamber
202
General Information
204
To Set up Your MSD for CI Operation
204
CI Maintenance
204
To Switch from the EI HES to the CI Source
205
To Remove the EI HES Radiator
206
To Connect/Disconnect Wiring to the EI HES Radiator
207
To Install the CI Source Radiator
209
To Switch from the CI Source to the EI HES
211
To Remove the CI Source Radiator
212
To Install the EI HES Radiator
214
To Switch from an EI XTR, SS, or Inert Source to the CI Source
215
To Switch from the CI Source to an EI XTR, SS, or Inert Source
216
To Remove the CI Source
217
To Connect/Disconnect Non-HES Model Wiring from the CI Source
218
To Connect/Disconnect EI HES Model Wiring to the CI Source
219
To Disassemble the CI Source
220
To Clean the CI Source
223
To Assemble the CI Source
226
To Remove the CI Source Filament
229
To Install a CI Source Filament
231
To Install the CI Source
232

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