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Hach MTC30101 User Instructions

Hach MTC30101 User Instructions

Refillable orp/redox electrode
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Refillable ORP/Redox electrode: MTC30101 or MTC30103
Safety Information
Precautionary Labels
Read all labels and tags attached to the instrument. Personal injury or damage to the
instrument could occur if not observed. A symbol, if noted on the instrument, will be included
with a danger or caution statement in the manual.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after
12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC),
European electrical equipment users must now return old or end-of life equipment to the Producer for disposal at no
charge to the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return
end-of-life equipment, producer-supplied electrical accessories, and all auxiliary items for proper disposal.
This is the safety alert symbol. Obey all safety messages that follow this symbol to avoid potential injury. If on the
instrument, refer to the instruction manual for operation or safety information.
Overview
The MTC30101 or MTC30103 is a refillable, combination oxidation reduction potential
(ORP/Redox) electrode with a built-in temperature sensor. The MTC30101 or MTC30103 is
available with a 1 or 3 meter cable and is intended for laboratory use. The electrode provides
ORP/Redox measurements in wastewater, drinking water and general applications. A 59 mL
bottle of reference electrolyte filling solution (3M KCl solution saturated with AgCl) is included
with the electrode.
Specifications
Specifications are subject to change without notice.
Specification
Electrode type
Range
Resolution
Temperature accuracy
Operating temperature range
Storage temperature range
Junction
Reference potential versus
Standard Hydrogen Electrode
Reference electrolyte
Fill solution
Reference type
Minimum sample depth
Dimensions
Cable connection
Warranty
User instructions
Details
Digital combination electrode with a refillable Ag/AgCl reference and a built-in
temperature sensor
± 1200 mV
0.1 mV
± 0.3 ºC (± 0.54 ºF)
0 to 80 °C
5 to 40 °C
Porous pin
207 mV at 25 ºC
Electrode filling solution, 3M KCl
3M KCl with saturated AgCl
Ag/AgCl (3M KCl)
20 mm
Diameter: 12 mm, Length: 103 mm, Total length: 200 mm, Cable length: 1 or 3 meter
Digital output and connector compatible with HQd meters
Sensor is covered by a 1 year warranty.
DOC272.53.80026
1

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Summary of Contents for Hach MTC30101

  • Page 1 The MTC30101 or MTC30103 is a refillable, combination oxidation reduction potential (ORP/Redox) electrode with a built-in temperature sensor. The MTC30101 or MTC30103 is available with a 1 or 3 meter cable and is intended for laboratory use. The electrode provides ORP/Redox measurements in wastewater, drinking water and general applications.
  • Page 2 4. Rinse the reference junction and platinum electrode with deionized water and blot dry with a lint-free cloth. 5. For temporary storage, fill the soaker bottle halfway with Hach Electrode Storage Solution or 3M KCl Filling Solution. Loosen the soaker bottle cap and push to install the soaker bottle on the electrode.
  • Page 3 Calibration notes • Probes are initially calibrated at the factory. However, regular calibration by the user is recommended for best measurement accuracy. • Additional standards can be selected in the MTC101 Calibration Options. • ZoBell’s redox potential is temperature dependent. The HQd calibration routine factors in this temperature dependency allowing accurate calibrations within the temperature range of 0 - 30 ºC.
  • Page 4 Run check standard The run check standard feature validates instrument performance between sample measurements. Use the run check standard feature for periodic or user-defined interval measurement of a traceable standard solution. Set the criteria for check standards from the MTC301 settings menu. Note: Access control must be off or a valid password entered before any of the check standard method options can be changed.
  • Page 5 Measurement–Direct Method Before measurement: The electrode must have the correct service-life time stamp. Set the date and time in the meter before attaching the electrode. The electrode is factory calibrated and ready for use. For applications that require greater accuracy and precision, verify the calibration with check standards or perform a user calibration. Routine calibrations are required (Calibration on page Make sure that the platinum electrode is clean before sample measurement...
  • Page 6 Measurement - conversion to SHE reference For some applications it is customary to report redox potential readings relative to the standard hydrogen electrode (SHE), also called normal hydrogen electrode (NHE). To do this, select the value in Table 1 Standard potential of reference electrode that corresponds to the temperature of the solution measured.
  • Page 7 1. Fill a 10 ml 2. Connect the 3. Pipet a 50 mL 4. Begin by adding 5. Plot the burette with a electrode to the sample into a titrant in 0.5 - 1 mL electrode potential standard titrant meter. 150-mL beaker.
  • Page 8 Long-term storage 1. Rinse the electrode with deionized water. Dry the electrode with a lint-free cloth. 2. Fill the electrode storage cap halfway with Hach Electrode Storage Solution or 3M potassium chloride (KCl) solution. 3. Install the electrode storage cap. Make sure that the storage cap covers the reference junction completely.
  • Page 9 Advanced operations Parameter-specific settings can be changed through the Full Access Options menu. Details about menu navigation, available options and how to change them are given in the screens, tables, and procedures throughout this section. The settings that can be changed are shown in Table Table 2 Parameter-specific settings Setting...
  • Page 10 Table 3 Measurement options settings Setting Options Description The response time affects the speed of the measurement by adjusting the stabilization criteria. Fast Response time Medium (default) Fast: 2 mV/min Slow Medium: 1 mV/min Slow: 0.5 mV/min The measurement limits can be set to match the acceptable Lower limit (default: -1200.0 values for the sample.
  • Page 11 Table 4 Calibration options settings Settings Option Description Offset must fall within set limits for Offset limits ± 1 mV - 250 mV (± 25 mV default) successful calibration. Enter standard value using up/down arrow keys. Custom standard value. Custom Standard value (for custom standard option) Range -1200.0 mV to 1200.0 mV...
  • Page 12 Probe requires Verify connectivity with another electrode or meter to service Damaged electrode confirm isolated issue with the electrode. Contact a Hach Technical Representative. Large number of methods stored on Continue to let probe connect. Do not disconnect probe. probe.
  • Page 13 Troubleshooting (continued) Message or Possible cause Action symptom Contaminated platinum disc Clean the electrode. Rinse reference junction holes with deionized water Clogged reference thoroughly and gently tap the electrode with hand or shake the electrode down to remove any air bubbles. Clean or condition the electrode and attempt recalibration.The electrode may not function correctly if the electrode has been left dry for extended periods of...
  • Page 14 Loveland, Colorado 80539-0389 U.S.A. International customers: Tel (800) -227-4224 (U.S.A. only) Tel +001 (970) 669-3050 Fax (970) 669-2932 Fax +001 (970) 669-2932 orders@hach.com • www.hach.com intl@hach.com © Hach Company, 2009. All rights reserved. Printed in the U.S.A. Edition 1 May 2009.

This manual is also suitable for:

Mtc30103