Knick Protos II 4400 User Manual
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Knick Protos II 4400 User Manual

Process analysis system
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Protos II 4400(X)
Process Analysis System
TAN Options
English
Device-specific add-on functions
for expanding functionality
7.00
25.3
pH
0.154
25.3
mS
cm
Time 10:26
Favorites menu
°C
°C
www.knick.de

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Summary of Contents for Knick Protos II 4400

  • Page 1 ® Protos II 4400(X) Process Analysis System TAN Options User Manual English Device-specific add-on functions for expanding functionality 7.00 25.3 °C 0.154 25.3 °C Time 10:26 Favorites menu Read before installation. Keep for future use. www.knick.de...
  • Page 2 The following registered trademarks are used in this manual without further marking: Calimatic® Protos® Sensocheck® Sensoface® are registered trademarks of Knick GmbH & Co. KG, Germany Memosens® is a registered trademark of Endress+Hauser Conducta GmbH & Co. KG, Germany Knick Elektronische Messgeräte GmbH & Co. KG, Germany...

  • Page 3: Table Of Contents

    Table of Contents How to Order an Add-On Function ..................5 Activating an Add-On Function .................... 6 FW4400-002: Buffer Table for pH Measurement ............. 7 FW4400-006: Current Characteristic ................... 8 FW4400-008: Ultrapure Water: Temperature Compensation (COND) ....10 FW4400-009: Concentration Determination (COND)..........11 FW4400-015: Oxygen Measurement ................18 Memory Card ..........................19 FW4400-102: 5 Parameter Sets ...................24...
  • Page 4 Protos II 4400(X)

  • Page 5: How To Order An Add-On Function

    How to Order an Add-On Function Add-on functions expand the device capabilities. The add-on functions are device-specific. When ordering an add-on function, you therefore have to specify the serial number of your FRONT module in addition to the respective order number. (The FRONT module contains the Protos system control).

  • Page 6: Activating An Add-On Function

    Set option to “Active”. Enter the TAN at 008 Cond TC Ultrapure Water Inactive the prompt. The current serial num- Inactive 009 Cond Concentration Inactive 015 Oxygen Measurement ber is shown. Back The option is available after the TAN has been entered. Protos II 4400(X)

  • Page 7: Fw4400-002: Buffer Table For Ph Measurement

    FW4400-002: Buffer Table for pH Measurement Parameter Setting/System Control/Buffer Table Specifying an Individual Buffer Set for pH Measurement You can enter an individual buffer set with 3 buffer solutions. To do so, enter the nominal buffer values for the correct temperature (0 ... 95 °C / 32 ... 203 °F, 5 °C/9 °F step size).

  • Page 8: Fw4400-006: Current Characteristic

    Meas. Value at 01 mA: ing to write down your adjustments. Meas. Value at 02 mA: pH 00.00 Meas. Value at 03 mA: pH 00.00 Meas. Value at 04 mA: pH 00.00 Meas. Value at 05 mA: pH 00.00 Back Protos II 4400(X)
  • Page 9 Current Characteristic Template Parameter Setting/BASE (OUT) Module/ Current Output/Characteristic: Table, own settings Measured values for process variable 00 mA ...._________ 01 mA ...._________ 02 mA ...._________ 03 mA ...._________ 04 mA ...._________ 05 mA ...._________ 06 mA ....

  • Page 10: Fw4400-008: Ultrapure Water: Temperature Compensation (Cond)

    4) Temp. Comp.: … Traces Select type of impurity: Back NaCl Neutral ultrapure water, for conductivity measurement in water processing behind gravel bed filter Acidic ultrapure water, for conductivity measurement behind cation filter Ammoniacal ultrapure water NaOH Alkaline ultrapure water Protos II 4400(X)

  • Page 11: Fw4400-009: Concentration Determination (Cond)

    FW4400-009: Concentration Determination (COND) Concentration Determination The substance concentration in percent by weight (wt%) is determined for , HNO , HCl, NaOH, NaCl, and Oleum. Conditions for Concentration Determination The following pages present the conductivity curves depending on substance concentration and medium temperature. The following conditions must be met for a reliable concentration determination: •...
  • Page 12 NaCl (0-28 %), HCl (0-18 %), NaOH (0-24 %), • Medium (“On” selected) (0-30%) (0-37 %), HNO (0-30 %), H (89-99 %), HCl (22-39 %), HNO (35-96 %), H (28-88 %), NaOH (15-50 %), Oleum (12-45%) Table Sulfuric acid H c [wt%] Protos II 4400(X)
  • Page 13 Nitric acid HNO c [wt%] Hydrochloric acid HCl c [wt%]...
  • Page 14 Sodium hydroxide solution NaOH c [wt%] Saline solution NaCl c [wt%] Protos II 4400(X)
  • Page 15 Oleum H •SO 120 °C 100 °C 85 °C 70 °C 55 °C 40 °C 25 °C 10 °C c [wt%]...
  • Page 16 Incorrect entries are marked with . Cond 4 at 015.0 °C 0.000 µS/cm Cond 5 at 020.0 °C 0.000 µS/cm Back The concentration table is selected in the menu: Parameter Setting/COND Module/Cal Presettings: Calibration mode: Automatic, Cal Solution: Table. Protos II 4400(X)
  • Page 17 The table is built up as 5 x 5 matrix: Concen- Concen- Concen- Concen- Concen- tration A tration B tration C tration D tration E Temp 1 Temp 2 Temp 3 Temp 4 Temp 5 Conditions for the Table: • The temperature values must be rising (Temp 1 is the lowest, Temp 5 the highest temperature).

  • Page 18: Fw4400-015: Oxygen Measurement

    FW4400-015: Oxygen Measurement For MS 4400(X)-160 Module Oxygen Measurement in the Saturation and ppb Range Add-on function FW4400(X)-015 enables amperometric Memosens oxygen sensors to be used in the saturation and ppb range. Protos II 4400(X)

  • Page 19: Memory Card

    See the information in the Safety Guide for Protos II 4400(X). Notes on Using the Memory Card The device must be opened to insert or replace the memory card.
  • Page 20 Connection to Computer Connect the memory card to the computer via a micro USB cable. Micro USB port Protos II 4400(X) system connection Note: Outside the hazardous location, the Ex memory card may be connected to a normal computer.
  • Page 21 Memory Card Card Types (ZU1080-P-*) Purpose Data Card (X) Records data Audit Trail Card (X) Records data with security option FW Update Card (X) Firmware update for function expansion FW Repair Card (X) Firmware repair in case of malfunction Custom FW Update Card Customer-specific FW versions Custom FW Repair Card Customer-specific FW versions...
  • Page 22 • Save: Save all device data on the Configuration Save Save Data Card Load • Load: Overwrite all device data with the data from the Data Card Back Note: Close Data Card before remov- ing (Maintenance menu) Protos II 4400(X)
  • Page 23 Memory Card Data Card: Save/Load Device Configuration Parameter Setting/System Control/Transfer Configuration. Saving/Loading the Complete Device Configuration “Save“ configuration means that the complete device configuration (except the passcode) is written on the Data Card. “Load” configuration means that the complete device configuration is read from the Data Card and programmed.

  • Page 24: Fw4400-102: 5 Parameter Sets

    (internal Save to 1 (Card) 1 (Card) 2 (Card) only) 3 (Card) 4 (Card) 5 (Card) Back Set 1 Set 2 Set B Data Card The parameter set is saved as a file on the Data Card. Protos II 4400(X)
  • Page 25 FW4400-102: 5 Parameter Sets Parameter Setting/System Control/Parameter Sets Menu Display Action Loading a Parameter Set from the Data Card Parameter Sets (Administrator) 1) Parameter Setting A,B (Internal) Parameter Sets 1,2 (Card) 2) System Control Save Parameter Set 1,2,3 (Card) Load Parameter Set 3) “Parameter Sets”...

  • Page 26: Fw4400-103: Measurement Recorder

    The zoom function is automatically switched on for fast changes. It begins sev- eral pixels before the event. This makes process variable fluctuation traceable in detail. Deleting Measurement Recorder Data Parameter Setting/System Control/Measurement Recorder: Clear Measurement Recorder: Yes. Press the “OK” softkey to confirm. Protos II 4400(X)
  • Page 27 FW4400-103: Measurement Recorder Parameter Setting/System Control/Memory Card/ Recording in Recorder: On Saving to Data Card Note: The device's internal memory has limited capacity and continuously overwrites the oldest data set after reaching maximum memory capacity. For recording sessions that take a long time, a data card is absolutely neces- sary.
  • Page 28 1st/2nd additional value and unit of measurement MAINT NAMUR signal* “Maintenance Required” HOLD NAMUR signal* “Function Check/HOLD” FAIL NAMUR signal* “Failure” * Term definition: NAMUR = German committee for measurement and control standards in the chemical industry Protos II 4400(X)

  • Page 29: Fw4400-104: Logbook

    FW4400-104: Logbook Parameter Setting/System Control/Logbook Saving to Data Card The logbook uses the FW4400-104 add-on function to record all entries in a file. When using the Data Card, 20,000 entries or more can be stored on the Data Card, depending on the memory load. Select menu: Parameter Setting/System Control/Memory Card/ Recording in Logbook On A new file is generated for each month.

  • Page 30: Fw4400-106: Firmware Update

    1) Switch off device 2) Place card in card slot 3) Switch on device 4) The automatic update process starts. Note: The firmware update add-on function need not be active for trouble- shooting with the FW Repair Card. Protos II 4400(X)
  • Page 31 Firmware Update: Save Firmware Parameter Setting/System Control/Firmware Update/Save Firmware Menu Display Action Save Firmware 1) Insert the FW Update Card. Option Activation (Administrator) 2) Select menu: Parameter Setting, 015 Oxygen Measurement Inactive Administrator Level 102 5 Parameter Sets Inactive 103 Measurement Recorder Inactive 3) Enter passcode.
  • Page 32 Start Back 6) Remove the memory card. Update Module Firmware A firmware update can also be carried out for specific modules. 1) Select “Update Module“. 2) Select a module. 3) Proceed as set out above. Protos II 4400(X)
  • Page 34 Knick Elektronische Messgeräte GmbH & Co. KG Headquarters Beuckestraße 22 • 14163 Berlin Germany Phone: +49 30 80191-0 Fax: +49 30 80191-200 info@knick.de www.knick.de Local Contacts www.knick-international.com Copyright 2019 • Subject to change Version: 9 This document was created on August 8, 2019.

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