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Summary of Contents for Dectris PILATUS 3 R 100K-M
- Page 1 Technical Specifications ® DECTRIS PILATUS 3 R 100KM Detector System Document Version v1.2.2 DECTRIS Ltd. 5405 Baden-Daettwil Switzerland www.dectris.com...
- Page 2 Document Version v1.2.2 © Copyright 2022 DECTRIS Ltd.
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Page 3: Table Of Contents
CONTENT CONTENT DOCUMENT HISTORY Current Document ........... Changes . - Page 4 OPERATION PROCEDURE Getting Started ..........27 Start-up Procedure .
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Page 5: Document History
DOCUMENT HISTORY Current Document Table 1: Current Version of this Document Version Date Status Prepared Checked Released v1.2.2 2022-09-05 release Changes Table 2: Changes to this Document Version Date Changes v1.2.2 2022-02-08 New Server O. v1.2.1 2020-09-15 Adjustment of Low Energy Options v1.2.0 2020-07-09 New Linux Distribution... -
Page 6: General Information
1. GENERAL INFORMATION 1.1. Contact and Support Address: DECTRIS Ltd. Taefernweg 1 5405 Baden-Daettwil Switzerland Phone: +41 56 500 21 02 Fax: +41 56 500 21 01 Homepage: http://www.dectris.com/ Email: support@dectris.com Should you have questions concerning the system or its use, please contact us via telephone, e-mail or fax. -
Page 7: Warranty Information
(in particular information, images or ® materials), unless otherwise indicated. Without the written permission of DECTRIS it is prohibited to integrate the protected contents in this publication into other programs or other websites or to use them by any other means. -
Page 8: Use Of The Pilatus3 R 100K-M
® We recycle DECTRIS detector systems that are no longer suitable for use. If you are not using your DECTRIS detector system any more, send it back to us. We will make sure that your system is responsibly and safely recycled. This is free for ®... -
Page 9: Technical Specifications
3. TECHNICAL SPECIFICATIONS 3.1. Specifications 3.1.1. Quantum Efficiency Table 3.1: Quantum Efficiency Sensor thickness 450 µm 1000 µm Quantum efficiency at 5.4 keV (Cr) 94 % > 80 % 8.0 keV (Cu) 98 % 96 % 17.5 keV (Mo) 47 % 76 % 3.1.2. -
Page 10: Power Supply Unit
Table 3.2: Technical Specifications - continued Readout time 7 ms Point-spread function 1 pixel (FWHM) Connection to control unit 1 x 1Gb Ethernet Power supply External power supply Data format (file writer) Raw data, TIF, EDF, CBF Software interface Through socket connection; Clients for EPICS, SPEC and stand-alone operation are available Dimensions (W x H x D) Detector Head: 114 mm x 69 mm x 118 mm,... -
Page 11: Ratings
3.2. Ratings 3.2.1. Detector Table 3.3: Power Ratings Detector power input +12 V DC, 30 W Fuse 4 A slow-blow fuse. Type: Schurter 5 mm x 20 mm, 4 A, 250 V AC Part No. 0001.2510 Warning Always replace fuses with the same type. Detector external trigger input 2.1 V to 5.0 V high level 0.0 V to 0.8 V low level... -
Page 12: Thermal Stabilization Unit
3.2.4. Thermal Stabilization Unit Table 3.6: Thermal Stabilization Unit Ratings Power input Single phase 100 VAC to 240 VAC, allowable voltage range ±10 %, 50/60 Hz, 8 A (100 VAC) to 3 A (240 VAC) Dimensions (W x H x D) 270 mm x 393 mm x 436 mm Weight 17.5 kg... -
Page 13: Vacuum Conditions For Detectors With Optional Vacuum Compatibility
Warning Only systems with a vacuum compatibility option are allowed to be operated in vacuum. Please contact support@dectris.com for information regarding vacuum compatibility upgrade. For in-vacuum operation of the detector following conditions must be fulfilled: Table 3.8: In-Vacuum Operating Conditions... -
Page 14: Detector Dimensions And Connectors
For in-vacuum applications electrical and cooling vacuum feedthrough sets (figure 4.4 and figure 4.5) are optionally available. Information ® 3D step files of the PILATUS3 R 100K-M detector are available on request. Please contact DECTRIS technical support for more information. (60) - Page 15 Without our agreement they may be neither copied ISO 2768 - mK 1 : 1 nor made accessible to a third party. ISO 13920 - BF DECTRIS LTD, 5400 Baden / Switzerland Document type: 162700.M.00.L01 Pilatus3 100K-M Vac. Outline.idw Created by...
- Page 16 ISO 2768 - mk Without our agreement they may be neither copied 1 : 2 nor made accessible to a third party. ISO 13920 - BF DECTRIS LTD, 5405 Baden-Daettwil / Switzerland Document type: 121400.M.80.L10 Electronics for P3 K-Systems.idw Created by...
- Page 17 POS-NR. PART NUMBER DESCRIPTION MATERIAL 1.4301 (X5CrNi18-10) 9210-D25-D50-ISO100-DEC Modifed Flange DN100 ISO-K 218-D50-SS 50 pin Sub-D Feedthrough Stainless Steel 218-D9-37-SS Sub-D Feedthrough Stainless Steel Bemerkungen (Remarks) Freimaßtoleranz Freimaßtoleranz Maßstab Rauheit (Rougness) europ.Projektion Funktionsmerkmale nach ISO/TS 16949 All informations provided in this drawing is considered to be confidential, proprietary and secret information.
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Page 18: Detector Head
4.1.2. Detector Head The detector head comes with a protective cover (1 mm, stainless steel) for the front window (figure 4.6), which should ® only be removed during operation (figure 4.7). The sensors are behind a 12 µm thick Mylar (PET) foil coated with 100 nm aluminium to protect them from humidity and ambient light. - Page 19 ® Removing the Mylar Window for Detectors with Optional Vacuum Compatibility For operation in vacuum and when the vacuum chamber is light-tight, the Mylar window is not required and can be re- ® moved for higher detection efficiency at low X-ray energies. The Mylar window can be removed by loosening four screws ®...
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Page 20: Detector Electronics Unit
Table 4.1: Connectors for cables/pipes on the detector head POWER Power cable (2m) to the detector electronics unit/vacuum feedthrough (grey or white D-Sub cable). DATA Data cable (2m) to the detector electronics unit/vacuum feedthrough (blue Samtec SQCD ribbon cable). DRY AIR Dry air or nitrogen for humidity control. -
Page 21: Vacuum Feedthroughs (Optional)
Table 4.3: Status LEDs on the detector back plane - continued Description TEMP Normally green. Turns red if the detector temperature or humidity is out of the limits. POWER Normally green. Turns red if there is a power failure or if the de- tector temperature or humidity is out of the limits. - Page 22 Caution The cable of the feedthrough set should not be combined with the default cables of the detector system. Figure 4.11: Picture of the optional PILATUS3 R 100K-M electrical vacuum feedthrough viewed from the vacuum (left) and air side (right). Figure 4.12: Picture of the optional PILATUS3 R 100K-M cooling vacuum feedthrough set with tubes through a standard DN40ISO-KF flange, and straight and elbow connectors for the detector head.
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Page 23: Detector Control Unit
4.2. Detector Control Unit 4.2.1. Configuration of the Detector Control Unit Please do not install or run any other software on the computer, except tools and software which are necessary for config- uring your data acquisition protocol. The detector control unit is set up with a standard installation of the CentOS 7.x distribution. Regular system updates can be made. -
Page 24: Samba Share
Table 4.5: Detector Control Unit Connectors - continued Connector Description EM2 (Embedded, figure 4.14) 1 GBase-T adapter Detector Interface Port1 labeled as Data Static 10.0.11.1 The start-up script /etc/rc.local disables ARP. Do not change this! Power (figure 4.14) AC Connector See DELL owner’s manual for further details. -
Page 25: In-Vacuum Operation For Detectors With Optional Vacuum Compatibility
Table 4.6: In-air operating conditions - continued Condition Definition Coolant 66 % distilled water 34 % ethylene glycol. Danger Ethylene glycol can be seriously harmful to your health or fatal if handled incorrectly. Consider the packaging and safefty instruc- tions provided by your local supplier. Information Before operating the thermal stabilization unit, please read the User Manual of the thermal stabilization unit. -
Page 26: Installing The Detector System Transport Considerations
5. INSTALLING THE DETECTOR SYSTEM 5.1. Transport Considerations Warning Avoid vibration and shock when moving the detector. The detector has been delivered in a robust transport box. Please keep this transport box for transport or storage purpose. 5.2. Mounting The detector can be mounted in the ways which are described below. 5.2.1. - Page 27 Figure 5.2: Drawing of the PILATUS3 R 100K-M Detector Head with extended Mounting Brackets (top view) Mounting the Detector Head from Below Warning It is strictly forbidden to add any threads to the detector base plate or to the detector housing. The detector should be mounted using the two internal M6x1 threads as shown in figure 5.3 (indicated with yellow circles).
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Page 28: Mounting The Detector Electronics Unit
Caution The four M6 screws must not intrude into the detector less than 10 mm and more than 15 mm. 5.2.2. Mounting the Detector Electronics Unit The detector electronics unit can be mounted from below using the four internal threads (M6x1). To mount the detector electronics unit from above, optional mounting brackets are available upon request. -
Page 29: In-Vacuum Use For Detectors With Optional Vacuum Compatibility
• Oil free, dry air of <20 % relative humidity or nitrogen must be used. −1 −1 • The recommended flow is 5 L h to 10 L h (at 2 bar). • For reliable operation we recommend dry air of <5 % relative humidity. •... -
Page 30: Mounting The Detector Control Unit
Figure 5.6: Examples of cooling connections for operation in vacuum. Depicted are horizontal (left) and vertical (right) connectors from the optional PILATUS3 R 100K-M cooling vacuum feedthrough set (section 4.1.4). 5.6. Mounting the Detector Control Unit Caution Make sure that the detector control unit has adequate ventilation. The detector control unit can be mounted in a standard 19 inch rack, which has to be properly grounded. -
Page 31: Temperature And Humidity Control
6. TEMPERATURE AND HUMIDITY CONTROL The PILATUS3 R 100K-M detector has a combined temperature and relative humidity sensor. The temperature and humid- ity control shuts down the detector when the relative humidity or the temperature of the sensor exceeds the limits in table 6.1. Table 6.1: Temperature and relative humidity limits Shutdown Temperature Shutdown Relative Humidity... -
Page 32: Operation Procedure
7. OPERATION PROCEDURE Before operating the detector, make sure you have read the Technical Specifications and the User Manual of the PILA- TUS3 R 100K-M detector. 7.1. Getting Started Before switching on: • Mount the detector head and the detector electronics unit properly. •... -
Page 33: Turning Off The Detector
7.3. Turning Off the Detector To turn off the detector: • Turn OFF the detector electronics unit power switch. • Do not remove the nitrogen/dry air connection. It is a requirement that it is left at the recommended flow rate according to section 5.4. -
Page 34: Storing The Detector
® ® The Mylar foil must not be touched or cleaned. If it becomes dirty or is damaged, please contact DECTRIS technical support. The housing can be cleaned with a soft tissue. Please refer to the user documentation of the thermal stabilization unit for detailed information about the maintenance of your thermal stabilization unit. -
Page 35: Troubleshooting
An overview of possible problems with the detector system and instructions in order to solve the problems is provided in table 8.1. If the problem you are experiencing is not listed below or if the instructions do not help, please contact support@dectris.com. Table 8.1: Troubleshooting... - Page 36 Check the status of the POWER LED. If it is red and the TEMP LED is green, there is a problem with the electronics – contact support@dectris.com. Detector housing is humid. Ambient humidity around the detector Shut down the detector immediately exceeds the operating conditions.
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Page 37: Certification Tests
9. CERTIFICATION TESTS The product is in conformity with the following standards: Table 9.1: Certification Tests for PILATUS3 R 100K-M EN 61000-6-2:2016 / IEC 61000-6-2:2005 (ed2.0), (industrial) EN 61000-6-4:2007 + A1:2011 / IEC 61000-6-4:2011 (ed2.1), (industrial) EN 61010-1:2010 / IEC 61010-1:2010 + AMD1:2016 EN 61326-1:2013 / IEC 61326-1:2012 (ed2.0) PILATUS3 R 100K-M Technical Specifications v1.2.2 32 | 34... - Page 38 ”DECTRIS INSTANT RETRIGGER”, ”DECTRIS MYTHEN”, ”DECTRIS PILATUS”, ”DECTRIS QUADRO”, ”DECTRIS SANTIS”, ”DECTRIS SÄNTIS”, ”DECTRIS SINGLA”, ”DECTRIS TITLIS”, ”DETECTING THE FUTURE” © 9/ 2022 DECTRIS Ltd., all rights reserved • Subject to technical modifications. PILATUS3 R 100K-M Technical Specifications v1.2.2 33 | 34...
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Page 39: Service Form
10. SERVICE FORM PILATUS3 R 100K-M Technical Specifications v1.2.2 34 | 34...
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